Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design

Pressurized hot water extraction (PHWE) could be a better alternative in enhancing the yield of valuable Citrus hystrix leaves essential oil. Thus, the fractional factorial design based on resolution V was used to assess the crucial factors that affect the essential oil yield (%Y) extracted from Cit...

Full description

Bibliographic Details
Main Authors: Abdul Halim, Noor Amirah, Zainal Abidin, Zurina, Siajam, Shamsul Izhar, Chong, Gun Hean, Harun, Mohd Razif
Format: Article
Published: Wiley 2020
_version_ 1825952379225243648
author Abdul Halim, Noor Amirah
Zainal Abidin, Zurina
Siajam, Shamsul Izhar
Chong, Gun Hean
Harun, Mohd Razif
author_facet Abdul Halim, Noor Amirah
Zainal Abidin, Zurina
Siajam, Shamsul Izhar
Chong, Gun Hean
Harun, Mohd Razif
author_sort Abdul Halim, Noor Amirah
collection UPM
description Pressurized hot water extraction (PHWE) could be a better alternative in enhancing the yield of valuable Citrus hystrix leaves essential oil. Thus, the fractional factorial design based on resolution V was used to assess the crucial factors that affect the essential oil yield (%Y) extracted from Citrus hystrix leaves through a PHWE. A maximum Y% of 1.63% was successfully isolated at conditions involving 0.08% moisture content, 1 mm particle size, 1:0.2 ml/g solvent-to-sample ratio, 30 min extraction time, and 120°C extraction temperature. Moisture content and particle size were the main effects that significantly affect the %Y, while the extraction time and solvent-to-sample ratio exhibited a moderate effect on %Y, followed by extraction temperature that showed the least effect on %Y. A developed regression model has shown good correlation and adequacy on %Y. Based on the compositional analysis, neoisopulegol hydrate appears to be the main constituents of the oil obtained.
first_indexed 2024-03-06T10:43:44Z
format Article
id upm.eprints-87536
institution Universiti Putra Malaysia
last_indexed 2024-03-06T10:43:44Z
publishDate 2020
publisher Wiley
record_format dspace
spelling upm.eprints-875362022-11-23T02:33:52Z http://psasir.upm.edu.my/id/eprint/87536/ Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design Abdul Halim, Noor Amirah Zainal Abidin, Zurina Siajam, Shamsul Izhar Chong, Gun Hean Harun, Mohd Razif Pressurized hot water extraction (PHWE) could be a better alternative in enhancing the yield of valuable Citrus hystrix leaves essential oil. Thus, the fractional factorial design based on resolution V was used to assess the crucial factors that affect the essential oil yield (%Y) extracted from Citrus hystrix leaves through a PHWE. A maximum Y% of 1.63% was successfully isolated at conditions involving 0.08% moisture content, 1 mm particle size, 1:0.2 ml/g solvent-to-sample ratio, 30 min extraction time, and 120°C extraction temperature. Moisture content and particle size were the main effects that significantly affect the %Y, while the extraction time and solvent-to-sample ratio exhibited a moderate effect on %Y, followed by extraction temperature that showed the least effect on %Y. A developed regression model has shown good correlation and adequacy on %Y. Based on the compositional analysis, neoisopulegol hydrate appears to be the main constituents of the oil obtained. Wiley 2020-09 Article PeerReviewed Abdul Halim, Noor Amirah and Zainal Abidin, Zurina and Siajam, Shamsul Izhar and Chong, Gun Hean and Harun, Mohd Razif (2020) Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design. Journal of Food Process Engineering, 43 (11). pp. 1-13. ISSN 1745-4530 https://onlinelibrary.wiley.com/doi/abs/10.1111/jfpe.13531 10.1111/jfpe.13531
spellingShingle Abdul Halim, Noor Amirah
Zainal Abidin, Zurina
Siajam, Shamsul Izhar
Chong, Gun Hean
Harun, Mohd Razif
Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design
title Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design
title_full Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design
title_fullStr Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design
title_full_unstemmed Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design
title_short Screening of factors influencing the yield of Citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution V fractional factorial design
title_sort screening of factors influencing the yield of citrus hystrix leaves essential oil extracted via pressurized hot water extraction based on resolution v fractional factorial design
work_keys_str_mv AT abdulhalimnooramirah screeningoffactorsinfluencingtheyieldofcitrushystrixleavesessentialoilextractedviapressurizedhotwaterextractionbasedonresolutionvfractionalfactorialdesign
AT zainalabidinzurina screeningoffactorsinfluencingtheyieldofcitrushystrixleavesessentialoilextractedviapressurizedhotwaterextractionbasedonresolutionvfractionalfactorialdesign
AT siajamshamsulizhar screeningoffactorsinfluencingtheyieldofcitrushystrixleavesessentialoilextractedviapressurizedhotwaterextractionbasedonresolutionvfractionalfactorialdesign
AT chonggunhean screeningoffactorsinfluencingtheyieldofcitrushystrixleavesessentialoilextractedviapressurizedhotwaterextractionbasedonresolutionvfractionalfactorialdesign
AT harunmohdrazif screeningoffactorsinfluencingtheyieldofcitrushystrixleavesessentialoilextractedviapressurizedhotwaterextractionbasedonresolutionvfractionalfactorialdesign