Optimization studies and compositional analysis of subcritical water extraction of essential oil from Citrus hystrix DC. leaves
Subcritical water extraction (SWE) of essential oil (EO) from Citrus hystrix DC. leaves was optimized using response surface methodology (RSM), involving factors of particle size (0.5–1) mm, sample-to-solvent ratio (0.025–0.175) g/mL, extraction temperature (140− 180) ◦C, and extraction time (20−...
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| Format: | Article |
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Elsevier BV
2021
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| _version_ | 1796982989975977984 |
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| author | Abdul Halim, Noor Amirah Zainal Abidin, Zurina Siajam, Shamsul Izhar Chong, Gun Hean Harun, Mohd Razif |
| author_facet | Abdul Halim, Noor Amirah Zainal Abidin, Zurina Siajam, Shamsul Izhar Chong, Gun Hean Harun, Mohd Razif |
| author_sort | Abdul Halim, Noor Amirah |
| collection | UPM |
| description | Subcritical water extraction (SWE) of essential oil (EO) from Citrus hystrix DC. leaves was optimized using
response surface methodology (RSM), involving factors of particle size (0.5–1) mm, sample-to-solvent ratio
(0.025–0.175) g/mL, extraction temperature (140− 180) ◦C, and extraction time (20− 40) minutes. Thus, an
optimal EO yield of (2.14 ± 0.03) % (w/w) was obtained at 0.75 mm, 0.025 g/mL, 174 ◦C, and 29 min. SWE was
found to yield significantly higher EO than the conventional hydrodistillation, within a shorter time. The
regression model was established, presenting a significant quadratic correlation (R2 = 0.97) and adequate for
predictions. SWE at 160 ◦C and 180 ◦C yielded 36 compounds, with isopulegol-dominant, exceeding SWE at
140 ◦C (21 compounds) and hydrodistillation (25 compounds). SWE with tunable temperatures not only
improved the quantity of EO but was also capable of enhancing the quality because more EO compounds were
extracted, offering diverse functionalities to nutraceutical sectors. |
| first_indexed | 2024-03-06T10:59:58Z |
| format | Article |
| id | upm.eprints-94465 |
| institution | Universiti Putra Malaysia |
| last_indexed | 2024-03-06T10:59:58Z |
| publishDate | 2021 |
| publisher | Elsevier BV |
| record_format | dspace |
| spelling | upm.eprints-944652023-02-07T03:50:02Z http://psasir.upm.edu.my/id/eprint/94465/ Optimization studies and compositional analysis of subcritical water extraction of essential oil from Citrus hystrix DC. leaves Abdul Halim, Noor Amirah Zainal Abidin, Zurina Siajam, Shamsul Izhar Chong, Gun Hean Harun, Mohd Razif Subcritical water extraction (SWE) of essential oil (EO) from Citrus hystrix DC. leaves was optimized using response surface methodology (RSM), involving factors of particle size (0.5–1) mm, sample-to-solvent ratio (0.025–0.175) g/mL, extraction temperature (140− 180) ◦C, and extraction time (20− 40) minutes. Thus, an optimal EO yield of (2.14 ± 0.03) % (w/w) was obtained at 0.75 mm, 0.025 g/mL, 174 ◦C, and 29 min. SWE was found to yield significantly higher EO than the conventional hydrodistillation, within a shorter time. The regression model was established, presenting a significant quadratic correlation (R2 = 0.97) and adequate for predictions. SWE at 160 ◦C and 180 ◦C yielded 36 compounds, with isopulegol-dominant, exceeding SWE at 140 ◦C (21 compounds) and hydrodistillation (25 compounds). SWE with tunable temperatures not only improved the quantity of EO but was also capable of enhancing the quality because more EO compounds were extracted, offering diverse functionalities to nutraceutical sectors. Elsevier BV 2021-08-18 Article PeerReviewed Abdul Halim, Noor Amirah and Zainal Abidin, Zurina and Siajam, Shamsul Izhar and Chong, Gun Hean and Harun, Mohd Razif (2021) Optimization studies and compositional analysis of subcritical water extraction of essential oil from Citrus hystrix DC. leaves. The Journal of Supercritical Fluids, 178. art. no. 105384. pp. 1-16. ISSN 0896-8446 https://www.sciencedirect.com/science/article/pii/S0896844621002266 10.1016/j.supflu.2021.105384 |
| spellingShingle | Abdul Halim, Noor Amirah Zainal Abidin, Zurina Siajam, Shamsul Izhar Chong, Gun Hean Harun, Mohd Razif Optimization studies and compositional analysis of subcritical water extraction of essential oil from Citrus hystrix DC. leaves |
| title | Optimization studies and compositional analysis of subcritical water extraction of essential oil from Citrus hystrix DC. leaves |
| title_full | Optimization studies and compositional analysis of subcritical water extraction of essential oil from Citrus hystrix DC. leaves |
| title_fullStr | Optimization studies and compositional analysis of subcritical water extraction of essential oil from Citrus hystrix DC. leaves |
| title_full_unstemmed | Optimization studies and compositional analysis of subcritical water extraction of essential oil from Citrus hystrix DC. leaves |
| title_short | Optimization studies and compositional analysis of subcritical water extraction of essential oil from Citrus hystrix DC. leaves |
| title_sort | optimization studies and compositional analysis of subcritical water extraction of essential oil from citrus hystrix dc leaves |
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