Formation of Nanotubular TiOa Bioactive Oxide Layer on Titanium and Cell Response Studies by

This work focus on the formation of titanium oxide {Ti02) nanotubes on theTi-6AI-4V alloy by anodization method in organic ethylene giycoi electrolyte (EG). The dimension of nancAubes could betuned by changing the electrochemical parameters such as NH4F content, voltage applied; and anodization ti...

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Main Authors: Sreekantan, Srimala, Ahmad, Zainal Arifin, Mat, Ishak, Mokhtar, Norehan
Format: Monograph
Published: Universiti Sains Malaysia 2011
Subjects:
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author Sreekantan, Srimala
Ahmad, Zainal Arifin
Mat, Ishak
Mokhtar, Norehan
author_facet Sreekantan, Srimala
Ahmad, Zainal Arifin
Mat, Ishak
Mokhtar, Norehan
author_sort Sreekantan, Srimala
collection USM
description This work focus on the formation of titanium oxide {Ti02) nanotubes on theTi-6AI-4V alloy by anodization method in organic ethylene giycoi electrolyte (EG). The dimension of nancAubes could betuned by changing the electrochemical parameters such as NH4F content, voltage applied; and anodization time. The average nanoporous or nonotube diameter and length were found to increase with increasing ambunt of fluoride, anodization voltage and anodization time. Minimum of 0.5 g NH4F is required for growth of nanotubes.:TT02 nanotubes with average diameter of 110 nm and 3.1 pm lengths were obtained in EG containing 0.7 g NH4F. Upon annealing from temperature 400°C to 600°C in argon atmosphere shows crystallization of the nanotubes to anatase phase exists at 400°C while rutile dominantly exists at eOO^C. Anodization in the organic electrolyte resulted in homogeneous structure unlike the one reported in aqueous acidified fluoride solution which resulted in inhomogeneous stnjcture due to the severe attack of the p-phase. For the case of behavior of cell interaction using human foreskin fibrobfast cells line (HS27) studies shown that amorphous Ti02 nanotubes structure has better cellular interaction as compare to anatase and rutile crystal structure
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spelling usm.eprints-376622022-09-21T08:29:36Z http://eprints.usm.my/37662/ Formation of Nanotubular TiOa Bioactive Oxide Layer on Titanium and Cell Response Studies by Sreekantan, Srimala Ahmad, Zainal Arifin Mat, Ishak Mokhtar, Norehan TN Mining Engineering. Metallurgy This work focus on the formation of titanium oxide {Ti02) nanotubes on theTi-6AI-4V alloy by anodization method in organic ethylene giycoi electrolyte (EG). The dimension of nancAubes could betuned by changing the electrochemical parameters such as NH4F content, voltage applied; and anodization time. The average nanoporous or nonotube diameter and length were found to increase with increasing ambunt of fluoride, anodization voltage and anodization time. Minimum of 0.5 g NH4F is required for growth of nanotubes.:TT02 nanotubes with average diameter of 110 nm and 3.1 pm lengths were obtained in EG containing 0.7 g NH4F. Upon annealing from temperature 400°C to 600°C in argon atmosphere shows crystallization of the nanotubes to anatase phase exists at 400°C while rutile dominantly exists at eOO^C. Anodization in the organic electrolyte resulted in homogeneous structure unlike the one reported in aqueous acidified fluoride solution which resulted in inhomogeneous stnjcture due to the severe attack of the p-phase. For the case of behavior of cell interaction using human foreskin fibrobfast cells line (HS27) studies shown that amorphous Ti02 nanotubes structure has better cellular interaction as compare to anatase and rutile crystal structure Universiti Sains Malaysia 2011 Monograph NonPeerReviewed Sreekantan, Srimala and Ahmad, Zainal Arifin and Mat, Ishak and Mokhtar, Norehan (2011) Formation of Nanotubular TiOa Bioactive Oxide Layer on Titanium and Cell Response Studies by. Project Report. Universiti Sains Malaysia. (Submitted)
spellingShingle TN Mining Engineering. Metallurgy
Sreekantan, Srimala
Ahmad, Zainal Arifin
Mat, Ishak
Mokhtar, Norehan
Formation of Nanotubular TiOa Bioactive Oxide Layer on Titanium and Cell Response Studies by
title Formation of Nanotubular TiOa Bioactive Oxide Layer on Titanium and Cell Response Studies by
title_full Formation of Nanotubular TiOa Bioactive Oxide Layer on Titanium and Cell Response Studies by
title_fullStr Formation of Nanotubular TiOa Bioactive Oxide Layer on Titanium and Cell Response Studies by
title_full_unstemmed Formation of Nanotubular TiOa Bioactive Oxide Layer on Titanium and Cell Response Studies by
title_short Formation of Nanotubular TiOa Bioactive Oxide Layer on Titanium and Cell Response Studies by
title_sort formation of nanotubular tioa bioactive oxide layer on titanium and cell response studies by
topic TN Mining Engineering. Metallurgy
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AT ahmadzainalarifin formationofnanotubulartioabioactiveoxidelayerontitaniumandcellresponsestudiesby
AT matishak formationofnanotubulartioabioactiveoxidelayerontitaniumandcellresponsestudiesby
AT mokhtarnorehan formationofnanotubulartioabioactiveoxidelayerontitaniumandcellresponsestudiesby