Crystal structure of 2-methyl-N-[(4-methylpyridin-2-yl)carbamothioyl]-benzamide
In the title compound, C15H15N3OS, there is an intramolecular N—H� � �O hydrogen bond and an intramolecular C—H� � �S hydrogen bond involving the C O and C S bonds which lie on opposite sides of the molecule. The molecule is non-planar with the benzene and pyridine rings being inclined to one a...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2015
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| Subjects: | |
| Online Access: | http://eprints.usm.my/38575/1/Crystal_structure_of_2-methyl-N-%5B%284-.pdf |
| _version_ | 1797010060015042560 |
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| author | Ameram, Nadiah Adam, Farook Fatihah, Nur Nadia Al-Juaid, Salih |
| author_facet | Ameram, Nadiah Adam, Farook Fatihah, Nur Nadia Al-Juaid, Salih |
| author_sort | Ameram, Nadiah |
| collection | USM |
| description | In the title compound, C15H15N3OS, there is an intramolecular
N—H� � �O hydrogen bond and an intramolecular C—H� � �S
hydrogen bond involving the C O and C S bonds which lie
on opposite sides of the molecule. The molecule is non-planar
with the benzene and pyridine rings being inclined to one
another by 26.86 (9)�. In the crystal, molecules are linked by
pairs of N—H� � �S hydrogen bonds, forming inversion dimers
with an R2
2(8) ring motif. The dimers are linked via C—H� � �S
hydrogen bonds, forming slabs parallel to the bc plane. |
| first_indexed | 2024-03-06T15:14:25Z |
| format | Article |
| id | usm.eprints-38575 |
| institution | Universiti Sains Malaysia |
| language | English |
| last_indexed | 2024-03-06T15:14:25Z |
| publishDate | 2015 |
| publisher | International Union of Crystallography |
| record_format | dspace |
| spelling | usm.eprints-385752018-01-26T07:49:51Z http://eprints.usm.my/38575/ Crystal structure of 2-methyl-N-[(4-methylpyridin-2-yl)carbamothioyl]-benzamide Ameram, Nadiah Adam, Farook Fatihah, Nur Nadia Al-Juaid, Salih QD1-999 Chemistry In the title compound, C15H15N3OS, there is an intramolecular N—H� � �O hydrogen bond and an intramolecular C—H� � �S hydrogen bond involving the C O and C S bonds which lie on opposite sides of the molecule. The molecule is non-planar with the benzene and pyridine rings being inclined to one another by 26.86 (9)�. In the crystal, molecules are linked by pairs of N—H� � �S hydrogen bonds, forming inversion dimers with an R2 2(8) ring motif. The dimers are linked via C—H� � �S hydrogen bonds, forming slabs parallel to the bc plane. International Union of Crystallography 2015 Article PeerReviewed application/pdf en http://eprints.usm.my/38575/1/Crystal_structure_of_2-methyl-N-%5B%284-.pdf Ameram, Nadiah and Adam, Farook and Fatihah, Nur Nadia and Al-Juaid, Salih (2015) Crystal structure of 2-methyl-N-[(4-methylpyridin-2-yl)carbamothioyl]-benzamide. Acta Crystallographica Section E: Crystallographic Communications, 71. 0356-0356. ISSN 2056-9890 (In Press) https://doi.org/10.1107/S2056989015007860 |
| spellingShingle | QD1-999 Chemistry Ameram, Nadiah Adam, Farook Fatihah, Nur Nadia Al-Juaid, Salih Crystal structure of 2-methyl-N-[(4-methylpyridin-2-yl)carbamothioyl]-benzamide |
| title | Crystal structure of 2-methyl-N-[(4-methylpyridin-2-yl)carbamothioyl]-benzamide |
| title_full | Crystal structure of 2-methyl-N-[(4-methylpyridin-2-yl)carbamothioyl]-benzamide |
| title_fullStr | Crystal structure of 2-methyl-N-[(4-methylpyridin-2-yl)carbamothioyl]-benzamide |
| title_full_unstemmed | Crystal structure of 2-methyl-N-[(4-methylpyridin-2-yl)carbamothioyl]-benzamide |
| title_short | Crystal structure of 2-methyl-N-[(4-methylpyridin-2-yl)carbamothioyl]-benzamide |
| title_sort | crystal structure of 2 methyl n 4 methylpyridin 2 yl carbamothioyl benzamide |
| topic | QD1-999 Chemistry |
| url | http://eprints.usm.my/38575/1/Crystal_structure_of_2-methyl-N-%5B%284-.pdf |
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