Synthesis And Characterization Of Graphene Filled Epoxy And Pedot Pss Composites

The discovery of graphene composites has driven changes among researchers because of their unique properties. The aim of the present study is to synthesize graphene and used as a filler in epoxy composites. The performance of synthesize graphene in epoxy was compared with commercialize graphene....

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Main Author: Arshad, Norshamira
Format: Thesis
Language:English
Published: 2018
Subjects:
Online Access:http://eprints.usm.my/46675/1/Synthesis%20And%20Characterization%20Of%20Graphene%20Filled%20Epoxy%20And%20Pedot%20Pss%20Composites.pdf
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author Arshad, Norshamira
author_facet Arshad, Norshamira
author_sort Arshad, Norshamira
collection USM
description The discovery of graphene composites has driven changes among researchers because of their unique properties. The aim of the present study is to synthesize graphene and used as a filler in epoxy composites. The performance of synthesize graphene in epoxy was compared with commercialize graphene. Graphene was synthesized using modified Hummer’s method and spin coating was used to produce epoxy composites with varying amount of filler loading. Analysis from Raman spectrum of synthesize graphene showed an increase in intensity ratio (ID/IG) which indicates the decrease of average size of the sp2 domains upon reduction of the GO. This is due to the loss of carbon formation. Besides that, FTIR spectra showed that the graphite has been successfully oxidized due to the presence of peak which referring to oxygencontaining groups. The best graphene filler loading in epoxy composites was obtained at 0.4vol% based on thermal conductivity measurement which indicate 37.5% increment compared to unfilled epoxy. Additionally, graphene/epoxy composites shows that the addition of filler in epoxy generally increase the electrical conductivity value from 7.38 x 10-6 to 7.19 x 10-5 S/cm, which is two order of magnitude higher than unfilled epoxy. Graphene/PEDOT:PSS with 1.0vol% loading exhibits 90% and 81% improvement in electrical and thermal conductivities, respectively compared to graphene/epoxy composite.
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spelling usm.eprints-466752021-11-17T03:42:13Z http://eprints.usm.my/46675/ Synthesis And Characterization Of Graphene Filled Epoxy And Pedot Pss Composites Arshad, Norshamira T Technology TA401-492 Materials of engineering and construction. Mechanics of materials The discovery of graphene composites has driven changes among researchers because of their unique properties. The aim of the present study is to synthesize graphene and used as a filler in epoxy composites. The performance of synthesize graphene in epoxy was compared with commercialize graphene. Graphene was synthesized using modified Hummer’s method and spin coating was used to produce epoxy composites with varying amount of filler loading. Analysis from Raman spectrum of synthesize graphene showed an increase in intensity ratio (ID/IG) which indicates the decrease of average size of the sp2 domains upon reduction of the GO. This is due to the loss of carbon formation. Besides that, FTIR spectra showed that the graphite has been successfully oxidized due to the presence of peak which referring to oxygencontaining groups. The best graphene filler loading in epoxy composites was obtained at 0.4vol% based on thermal conductivity measurement which indicate 37.5% increment compared to unfilled epoxy. Additionally, graphene/epoxy composites shows that the addition of filler in epoxy generally increase the electrical conductivity value from 7.38 x 10-6 to 7.19 x 10-5 S/cm, which is two order of magnitude higher than unfilled epoxy. Graphene/PEDOT:PSS with 1.0vol% loading exhibits 90% and 81% improvement in electrical and thermal conductivities, respectively compared to graphene/epoxy composite. 2018-09-01 Thesis NonPeerReviewed application/pdf en http://eprints.usm.my/46675/1/Synthesis%20And%20Characterization%20Of%20Graphene%20Filled%20Epoxy%20And%20Pedot%20Pss%20Composites.pdf Arshad, Norshamira (2018) Synthesis And Characterization Of Graphene Filled Epoxy And Pedot Pss Composites. Masters thesis, Universiti Sains Malaysia.
spellingShingle T Technology
TA401-492 Materials of engineering and construction. Mechanics of materials
Arshad, Norshamira
Synthesis And Characterization Of Graphene Filled Epoxy And Pedot Pss Composites
title Synthesis And Characterization Of Graphene Filled Epoxy And Pedot Pss Composites
title_full Synthesis And Characterization Of Graphene Filled Epoxy And Pedot Pss Composites
title_fullStr Synthesis And Characterization Of Graphene Filled Epoxy And Pedot Pss Composites
title_full_unstemmed Synthesis And Characterization Of Graphene Filled Epoxy And Pedot Pss Composites
title_short Synthesis And Characterization Of Graphene Filled Epoxy And Pedot Pss Composites
title_sort synthesis and characterization of graphene filled epoxy and pedot pss composites
topic T Technology
TA401-492 Materials of engineering and construction. Mechanics of materials
url http://eprints.usm.my/46675/1/Synthesis%20And%20Characterization%20Of%20Graphene%20Filled%20Epoxy%20And%20Pedot%20Pss%20Composites.pdf
work_keys_str_mv AT arshadnorshamira synthesisandcharacterizationofgraphenefilledepoxyandpedotpsscomposites