Effect Of ZnO Seed Layer On The Growth Of ZnO Nanorods Via Solution Precipitation Method

There are various types of substrates that have been used to grow ZnO nanorods on the surface. However, it is difficult to obtain highly aligned ZnO nanorods on Si substrate because of the large mismatches between ZnO and Si. This problem could be addressed by depositing a highly (002) oriented ZnO...

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Tác giả chính: Nik Jusoh, Nik Anis Hafiza
Định dạng: Monograph
Ngôn ngữ:English
Được phát hành: Universiti Sains Malaysia 2018
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Truy cập trực tuyến:http://eprints.usm.my/53053/1/Effect%20Of%20ZnO%20Seed%20Layer%20On%20The%20Growth%20Of%20ZnO%20Nanorods%20Via%20Solution%20Precipitation%20Method_Nik%20Anis%20Hafiza%20Nik%20Jusoh_B1_2018.pdf
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author Nik Jusoh, Nik Anis Hafiza
author_facet Nik Jusoh, Nik Anis Hafiza
author_sort Nik Jusoh, Nik Anis Hafiza
collection USM
description There are various types of substrates that have been used to grow ZnO nanorods on the surface. However, it is difficult to obtain highly aligned ZnO nanorods on Si substrate because of the large mismatches between ZnO and Si. This problem could be addressed by depositing a highly (002) oriented ZnO seed layer on the surface of Si substrate. The seed layer of ZnO improved the coverage and aligned growth of ZnO nanorods. In this project, ZnO seed layers were deposited on the Si substrate using spin coating followed by post annealing in air. The precursors were zinc acetate dihydrate dissolved in ethanol. The deposition of the seed layer was done at different cycles of coating and different rotational speed (rpm) to improve the coverage of ZnO nanorods.The SEM images shows that the highest number of coating cycles (11 cycles) and lowest rpm (1000 rpm) has the best ZnO nanorods surface coverage on the substrate. For 1000 rpm, the percentage of ZnO nanorods surface coverage is 82.2%, while for 1000rpm at 11 coating cycles was 84.42%. The result showed that the lowest speed and highest number of coating cycles provided the best coverage of ZnO seed layer. Next, ZnO nanorods were synthesized from the pre-deposited ZnO seed layer via solution precipitation method. Different annealing temperatures on the ZnO seed layer were conducted to observe the differences of the alignment. The ZnO nanorods grown at 350oC showed the best vertical alignment as the nanorods grew at c-axis.
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spelling usm.eprints-530532022-06-24T09:33:52Z http://eprints.usm.my/53053/ Effect Of ZnO Seed Layer On The Growth Of ZnO Nanorods Via Solution Precipitation Method Nik Jusoh, Nik Anis Hafiza T Technology TN Mining Engineering. Metallurgy There are various types of substrates that have been used to grow ZnO nanorods on the surface. However, it is difficult to obtain highly aligned ZnO nanorods on Si substrate because of the large mismatches between ZnO and Si. This problem could be addressed by depositing a highly (002) oriented ZnO seed layer on the surface of Si substrate. The seed layer of ZnO improved the coverage and aligned growth of ZnO nanorods. In this project, ZnO seed layers were deposited on the Si substrate using spin coating followed by post annealing in air. The precursors were zinc acetate dihydrate dissolved in ethanol. The deposition of the seed layer was done at different cycles of coating and different rotational speed (rpm) to improve the coverage of ZnO nanorods.The SEM images shows that the highest number of coating cycles (11 cycles) and lowest rpm (1000 rpm) has the best ZnO nanorods surface coverage on the substrate. For 1000 rpm, the percentage of ZnO nanorods surface coverage is 82.2%, while for 1000rpm at 11 coating cycles was 84.42%. The result showed that the lowest speed and highest number of coating cycles provided the best coverage of ZnO seed layer. Next, ZnO nanorods were synthesized from the pre-deposited ZnO seed layer via solution precipitation method. Different annealing temperatures on the ZnO seed layer were conducted to observe the differences of the alignment. The ZnO nanorods grown at 350oC showed the best vertical alignment as the nanorods grew at c-axis. Universiti Sains Malaysia 2018-06-01 Monograph NonPeerReviewed application/pdf en http://eprints.usm.my/53053/1/Effect%20Of%20ZnO%20Seed%20Layer%20On%20The%20Growth%20Of%20ZnO%20Nanorods%20Via%20Solution%20Precipitation%20Method_Nik%20Anis%20Hafiza%20Nik%20Jusoh_B1_2018.pdf Nik Jusoh, Nik Anis Hafiza (2018) Effect Of ZnO Seed Layer On The Growth Of ZnO Nanorods Via Solution Precipitation Method. Project Report. Universiti Sains Malaysia, Pusat Pengajian Kejuruteraan Bahan dan Sumber Mineral. (Submitted)
spellingShingle T Technology
TN Mining Engineering. Metallurgy
Nik Jusoh, Nik Anis Hafiza
Effect Of ZnO Seed Layer On The Growth Of ZnO Nanorods Via Solution Precipitation Method
title Effect Of ZnO Seed Layer On The Growth Of ZnO Nanorods Via Solution Precipitation Method
title_full Effect Of ZnO Seed Layer On The Growth Of ZnO Nanorods Via Solution Precipitation Method
title_fullStr Effect Of ZnO Seed Layer On The Growth Of ZnO Nanorods Via Solution Precipitation Method
title_full_unstemmed Effect Of ZnO Seed Layer On The Growth Of ZnO Nanorods Via Solution Precipitation Method
title_short Effect Of ZnO Seed Layer On The Growth Of ZnO Nanorods Via Solution Precipitation Method
title_sort effect of zno seed layer on the growth of zno nanorods via solution precipitation method
topic T Technology
TN Mining Engineering. Metallurgy
url http://eprints.usm.my/53053/1/Effect%20Of%20ZnO%20Seed%20Layer%20On%20The%20Growth%20Of%20ZnO%20Nanorods%20Via%20Solution%20Precipitation%20Method_Nik%20Anis%20Hafiza%20Nik%20Jusoh_B1_2018.pdf
work_keys_str_mv AT nikjusohnikanishafiza effectofznoseedlayeronthegrowthofznonanorodsviasolutionprecipitationmethod