Green Synthesis Of Silver Nanoparticles Using Curcuma Xanthorrhiza Rhizome Extract

The employment of plant extract in the synthesis process of silver nanoparticles is the recent advancement in green chemistry and garnering great interest among researchers worldwide. This study mainly emphasizes on green synthesis of silver nanoparticles using Curcuma xanthorrhiza (C. xanthorrhiz...

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Main Author: Deva, Nathan
Format: Monograph
Language:English
Published: Universiti Sains Malaysia 2021
Subjects:
Online Access:http://eprints.usm.my/54505/1/Green%20Synthesis%20Of%20Silver%20Nanoparticles%20Using%20Curcuma%20Xanthorrhiza%20Rhizome%20Extract_Nathan%20Deva_K4_2021_ESAR.pdf
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author Deva, Nathan
author_facet Deva, Nathan
author_sort Deva, Nathan
collection USM
description The employment of plant extract in the synthesis process of silver nanoparticles is the recent advancement in green chemistry and garnering great interest among researchers worldwide. This study mainly emphasizes on green synthesis of silver nanoparticles using Curcuma xanthorrhiza (C. xanthorrhiza) rhizome extract, which acts as a reducing and capping agent. Silver ions in the silver nitrate solution can be reduced into zero valence silver nanoparticles when the rhizome extract is mixed. The reduction of silver ions resulted in color changes in the mixture from yellow to dark brown due to the surface plasmon resonance (SPR) phenomenon. Thus, several parameters influencing the green synthesis of silver nanoparticles were optimized by manipulating variables in the experiment. Then, the synthesized silver nanoparticles were characterized via analytical equipment such as UV-Visible spectrometer and Energy Dispersive X-ray (EDX) spectrometer. The UV-Vis spectrum of the silver nanoparticles was obtained, and the maximum absorption peak was acquired at a wavelength in the range of 445 to 450 nm. Hence, the best conditions for synthesizing silver nanoparticles were determined and found to be 8 wt % rhizome extract concentration, 8 mM silver nitrate solution concentration, 1:5 rhizome extract to silver nitrate solution volume ratio, and 72 hours of incubation time. Furthermore, the EDX analysis of silver nanoparticles demonstrated a spectrum of elemental composition in which silver has the highest peak at 3 keV. Several other compounds in the spectrum indicate the presence of biomolecules from the extract on the surface of nanoparticles as a stabilizing agent. These results showed that the reduction process of silver ions using C. xanthorrhiza rhizome extract is a greener method with less toxicity and can form more refined and stable nanoparticles.
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spelling usm.eprints-545052022-09-06T07:12:13Z http://eprints.usm.my/54505/ Green Synthesis Of Silver Nanoparticles Using Curcuma Xanthorrhiza Rhizome Extract Deva, Nathan T Technology TP Chemical Technology The employment of plant extract in the synthesis process of silver nanoparticles is the recent advancement in green chemistry and garnering great interest among researchers worldwide. This study mainly emphasizes on green synthesis of silver nanoparticles using Curcuma xanthorrhiza (C. xanthorrhiza) rhizome extract, which acts as a reducing and capping agent. Silver ions in the silver nitrate solution can be reduced into zero valence silver nanoparticles when the rhizome extract is mixed. The reduction of silver ions resulted in color changes in the mixture from yellow to dark brown due to the surface plasmon resonance (SPR) phenomenon. Thus, several parameters influencing the green synthesis of silver nanoparticles were optimized by manipulating variables in the experiment. Then, the synthesized silver nanoparticles were characterized via analytical equipment such as UV-Visible spectrometer and Energy Dispersive X-ray (EDX) spectrometer. The UV-Vis spectrum of the silver nanoparticles was obtained, and the maximum absorption peak was acquired at a wavelength in the range of 445 to 450 nm. Hence, the best conditions for synthesizing silver nanoparticles were determined and found to be 8 wt % rhizome extract concentration, 8 mM silver nitrate solution concentration, 1:5 rhizome extract to silver nitrate solution volume ratio, and 72 hours of incubation time. Furthermore, the EDX analysis of silver nanoparticles demonstrated a spectrum of elemental composition in which silver has the highest peak at 3 keV. Several other compounds in the spectrum indicate the presence of biomolecules from the extract on the surface of nanoparticles as a stabilizing agent. These results showed that the reduction process of silver ions using C. xanthorrhiza rhizome extract is a greener method with less toxicity and can form more refined and stable nanoparticles. Universiti Sains Malaysia 2021-06-14 Monograph NonPeerReviewed application/pdf en http://eprints.usm.my/54505/1/Green%20Synthesis%20Of%20Silver%20Nanoparticles%20Using%20Curcuma%20Xanthorrhiza%20Rhizome%20Extract_Nathan%20Deva_K4_2021_ESAR.pdf Deva, Nathan (2021) Green Synthesis Of Silver Nanoparticles Using Curcuma Xanthorrhiza Rhizome Extract. Project Report. Universiti Sains Malaysia, Pusat Pengajian Kejuruteraan Kimia. (Submitted)
spellingShingle T Technology
TP Chemical Technology
Deva, Nathan
Green Synthesis Of Silver Nanoparticles Using Curcuma Xanthorrhiza Rhizome Extract
title Green Synthesis Of Silver Nanoparticles Using Curcuma Xanthorrhiza Rhizome Extract
title_full Green Synthesis Of Silver Nanoparticles Using Curcuma Xanthorrhiza Rhizome Extract
title_fullStr Green Synthesis Of Silver Nanoparticles Using Curcuma Xanthorrhiza Rhizome Extract
title_full_unstemmed Green Synthesis Of Silver Nanoparticles Using Curcuma Xanthorrhiza Rhizome Extract
title_short Green Synthesis Of Silver Nanoparticles Using Curcuma Xanthorrhiza Rhizome Extract
title_sort green synthesis of silver nanoparticles using curcuma xanthorrhiza rhizome extract
topic T Technology
TP Chemical Technology
url http://eprints.usm.my/54505/1/Green%20Synthesis%20Of%20Silver%20Nanoparticles%20Using%20Curcuma%20Xanthorrhiza%20Rhizome%20Extract_Nathan%20Deva_K4_2021_ESAR.pdf
work_keys_str_mv AT devanathan greensynthesisofsilvernanoparticlesusingcurcumaxanthorrhizarhizomeextract