Preliminary Study Of Self-Setting 45S5 Bioglass Granular Cement

The objectives of this study is to investigate the effect of different concentration ofacidic calcium phosphate solution and soaking time on the 45S5 bioglass granular cement. The acidic calcium phosphate solution contain different concentration of MCPM (25 mmol/L, 50 mmol/L, 75 mmol/L and 100mmol/...

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Main Author: Imbau, Arnold
Format: Monograph
Language:English
Published: Universiti Sains Malaysia 2022
Subjects:
Online Access:http://eprints.usm.my/56436/1/Preliminary%20Study%20Of%20Self-Setting%2045S5%20Bioglass%20Granular%20Cement_%20Arnold%20Imbau.pdf
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author Imbau, Arnold
author_facet Imbau, Arnold
author_sort Imbau, Arnold
collection USM
description The objectives of this study is to investigate the effect of different concentration ofacidic calcium phosphate solution and soaking time on the 45S5 bioglass granular cement. The acidic calcium phosphate solution contain different concentration of MCPM (25 mmol/L, 50 mmol/L, 75 mmol/L and 100mmol/L) were imposed to 45S5 bioglass granules at temperature of 25°C (for 2, 4, 6 and 8 hours) to see its setting ability. Several characterization methods such as XRD, SEM, FTIR, measurement of pH value and compression test were carried out on 45S5 bioglass granular cement in order to understand its setting properties. XRD and SEM analysis result showed that the DCPD crystal are present and bridging to each other between the surface of 45S5 bioglass granular cement. The DCPD crystal that are form were increased when the concentration of acidic calcium phosphate is increased. Moreover, this study also shows the pH value of 45S5 bioglass granular cement that has been soak for 8 hours with acidic calcium phosphate solution are low after the specimen are immersed into HBSS solution for 1 day. On the other hand, this study also shows the compression strength for the specimen that are fully set at 8 hours of soaking time with acidic calcium phosphate solution with concentration of MCPM 100 mmol/L is 0.116 Mpa. Therefore, this study proved that the effect of concentration acidic calcium phosphate solution and the soaking time able to set the 45S5 bioglass granular at temperature 25°C.
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spelling usm.eprints-564362023-01-19T09:23:12Z http://eprints.usm.my/56436/ Preliminary Study Of Self-Setting 45S5 Bioglass Granular Cement Imbau, Arnold T Technology TN Mining Engineering. Metallurgy The objectives of this study is to investigate the effect of different concentration ofacidic calcium phosphate solution and soaking time on the 45S5 bioglass granular cement. The acidic calcium phosphate solution contain different concentration of MCPM (25 mmol/L, 50 mmol/L, 75 mmol/L and 100mmol/L) were imposed to 45S5 bioglass granules at temperature of 25°C (for 2, 4, 6 and 8 hours) to see its setting ability. Several characterization methods such as XRD, SEM, FTIR, measurement of pH value and compression test were carried out on 45S5 bioglass granular cement in order to understand its setting properties. XRD and SEM analysis result showed that the DCPD crystal are present and bridging to each other between the surface of 45S5 bioglass granular cement. The DCPD crystal that are form were increased when the concentration of acidic calcium phosphate is increased. Moreover, this study also shows the pH value of 45S5 bioglass granular cement that has been soak for 8 hours with acidic calcium phosphate solution are low after the specimen are immersed into HBSS solution for 1 day. On the other hand, this study also shows the compression strength for the specimen that are fully set at 8 hours of soaking time with acidic calcium phosphate solution with concentration of MCPM 100 mmol/L is 0.116 Mpa. Therefore, this study proved that the effect of concentration acidic calcium phosphate solution and the soaking time able to set the 45S5 bioglass granular at temperature 25°C. Universiti Sains Malaysia 2022-08-01 Monograph NonPeerReviewed application/pdf en http://eprints.usm.my/56436/1/Preliminary%20Study%20Of%20Self-Setting%2045S5%20Bioglass%20Granular%20Cement_%20Arnold%20Imbau.pdf Imbau, Arnold (2022) Preliminary Study Of Self-Setting 45S5 Bioglass Granular Cement. Project Report. Universiti Sains Malaysia, Pusat Pengajian Kejuruteraan Bahan dan Sumber Mineral. (Submitted)
spellingShingle T Technology
TN Mining Engineering. Metallurgy
Imbau, Arnold
Preliminary Study Of Self-Setting 45S5 Bioglass Granular Cement
title Preliminary Study Of Self-Setting 45S5 Bioglass Granular Cement
title_full Preliminary Study Of Self-Setting 45S5 Bioglass Granular Cement
title_fullStr Preliminary Study Of Self-Setting 45S5 Bioglass Granular Cement
title_full_unstemmed Preliminary Study Of Self-Setting 45S5 Bioglass Granular Cement
title_short Preliminary Study Of Self-Setting 45S5 Bioglass Granular Cement
title_sort preliminary study of self setting 45s5 bioglass granular cement
topic T Technology
TN Mining Engineering. Metallurgy
url http://eprints.usm.my/56436/1/Preliminary%20Study%20Of%20Self-Setting%2045S5%20Bioglass%20Granular%20Cement_%20Arnold%20Imbau.pdf
work_keys_str_mv AT imbauarnold preliminarystudyofselfsetting45s5bioglassgranularcement