The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method

In this present work, hydrosodalite was successfully synthesized by hydrothermal method from the raw Johor kaolin, Malaysia. In order to get the size that was less than 63 lm, the raw kaolin was ground and sieved. Since the raw kaolin did not undergo the beneficiation process, thus the raw kaolin...

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Main Authors: Sazali, Norsuhailizah, Harun, Zawati, Azhar, Faiz Hafeez, Bahri, Syamsutajri Syamsol, Raja Ahmad, Raja Puteri Nurul Adibah, Hussin@Isa, Rosniza, Misdan, Nurasyikin
Format: Article
Language:English
Published: Elsevier 2021
Subjects:
Online Access:http://eprints.uthm.edu.my/6644/1/P13067_f086c1fd022be8be32b84fad851d59e1.pdf
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author Sazali, Norsuhailizah
Harun, Zawati
Azhar, Faiz Hafeez
Bahri, Syamsutajri Syamsol
Raja Ahmad, Raja Puteri Nurul Adibah
Hussin@Isa, Rosniza
Misdan, Nurasyikin
author_facet Sazali, Norsuhailizah
Harun, Zawati
Azhar, Faiz Hafeez
Bahri, Syamsutajri Syamsol
Raja Ahmad, Raja Puteri Nurul Adibah
Hussin@Isa, Rosniza
Misdan, Nurasyikin
author_sort Sazali, Norsuhailizah
collection UTHM
description In this present work, hydrosodalite was successfully synthesized by hydrothermal method from the raw Johor kaolin, Malaysia. In order to get the size that was less than 63 lm, the raw kaolin was ground and sieved. Since the raw kaolin did not undergo the beneficiation process, thus the raw kaolin then was calcinated for four hours at 650 �C to produce more reactive clay (metakaolin). The synthesizing of hydrosodalite form of the metakaolin powder was conducted by mixing the powder with different molar�ities of sodium hydroxide, NaOH. This mixture was further treated by soaking it at a temperature of 40 �C for 24 h. The reaction mixture was then moved for 12 h into the autoclave for the 100 �C under hydrother�mal conditions. The results through phase analysis via XRD, microstructure observation via SEM and bonding analysis via FTIR has revealed the existence of hydrosodalite phase in comparison with pure kao�lin and metakaolin. The result also indicated the lower NaOH (4 M) molarity gave a higher percentage of hydrosodalite formation in comparison with higher molarity of NaOH at 5 M, 6 M and 7 M.
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spelling uthm.eprints-66442022-03-14T01:26:28Z http://eprints.uthm.edu.my/6644/ The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method Sazali, Norsuhailizah Harun, Zawati Azhar, Faiz Hafeez Bahri, Syamsutajri Syamsol Raja Ahmad, Raja Puteri Nurul Adibah Hussin@Isa, Rosniza Misdan, Nurasyikin TJ Mechanical engineering and machinery In this present work, hydrosodalite was successfully synthesized by hydrothermal method from the raw Johor kaolin, Malaysia. In order to get the size that was less than 63 lm, the raw kaolin was ground and sieved. Since the raw kaolin did not undergo the beneficiation process, thus the raw kaolin then was calcinated for four hours at 650 �C to produce more reactive clay (metakaolin). The synthesizing of hydrosodalite form of the metakaolin powder was conducted by mixing the powder with different molar�ities of sodium hydroxide, NaOH. This mixture was further treated by soaking it at a temperature of 40 �C for 24 h. The reaction mixture was then moved for 12 h into the autoclave for the 100 �C under hydrother�mal conditions. The results through phase analysis via XRD, microstructure observation via SEM and bonding analysis via FTIR has revealed the existence of hydrosodalite phase in comparison with pure kao�lin and metakaolin. The result also indicated the lower NaOH (4 M) molarity gave a higher percentage of hydrosodalite formation in comparison with higher molarity of NaOH at 5 M, 6 M and 7 M. Elsevier 2021 Article PeerReviewed text en http://eprints.uthm.edu.my/6644/1/P13067_f086c1fd022be8be32b84fad851d59e1.pdf Sazali, Norsuhailizah and Harun, Zawati and Azhar, Faiz Hafeez and Bahri, Syamsutajri Syamsol and Raja Ahmad, Raja Puteri Nurul Adibah and Hussin@Isa, Rosniza and Misdan, Nurasyikin (2021) The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method. Materials Today: Proceedings, 46. pp. 2045-2051. https://doi.org/10.1016/j.matpr.2021.03.135
spellingShingle TJ Mechanical engineering and machinery
Sazali, Norsuhailizah
Harun, Zawati
Azhar, Faiz Hafeez
Bahri, Syamsutajri Syamsol
Raja Ahmad, Raja Puteri Nurul Adibah
Hussin@Isa, Rosniza
Misdan, Nurasyikin
The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method
title The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method
title_full The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method
title_fullStr The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method
title_full_unstemmed The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method
title_short The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method
title_sort effect of various molarity sodium hydroxide naoh on the hydrosodalite formation from synthesis of johor kaolin malaysia by hydrothermal method
topic TJ Mechanical engineering and machinery
url http://eprints.uthm.edu.my/6644/1/P13067_f086c1fd022be8be32b84fad851d59e1.pdf
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