The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method
In this present work, hydrosodalite was successfully synthesized by hydrothermal method from the raw Johor kaolin, Malaysia. In order to get the size that was less than 63 lm, the raw kaolin was ground and sieved. Since the raw kaolin did not undergo the beneficiation process, thus the raw kaolin...
Autores principales: | , , , , , , |
---|---|
Formato: | Artículo |
Lenguaje: | English |
Publicado: |
Elsevier
2021
|
Materias: | |
Acceso en línea: | http://eprints.uthm.edu.my/6644/1/P13067_f086c1fd022be8be32b84fad851d59e1.pdf |
_version_ | 1825710226442027008 |
---|---|
author | Sazali, Norsuhailizah Harun, Zawati Azhar, Faiz Hafeez Bahri, Syamsutajri Syamsol Raja Ahmad, Raja Puteri Nurul Adibah Hussin@Isa, Rosniza Misdan, Nurasyikin |
author_facet | Sazali, Norsuhailizah Harun, Zawati Azhar, Faiz Hafeez Bahri, Syamsutajri Syamsol Raja Ahmad, Raja Puteri Nurul Adibah Hussin@Isa, Rosniza Misdan, Nurasyikin |
author_sort | Sazali, Norsuhailizah |
collection | UTHM |
description | In this present work, hydrosodalite was successfully synthesized by hydrothermal method from the raw
Johor kaolin, Malaysia. In order to get the size that was less than 63 lm, the raw kaolin was ground and
sieved. Since the raw kaolin did not undergo the beneficiation process, thus the raw kaolin then was
calcinated for four hours at 650 �C to produce more reactive clay (metakaolin). The synthesizing of
hydrosodalite form of the metakaolin powder was conducted by mixing the powder with different molar�ities of sodium hydroxide, NaOH. This mixture was further treated by soaking it at a temperature of 40 �C
for 24 h. The reaction mixture was then moved for 12 h into the autoclave for the 100 �C under hydrother�mal conditions. The results through phase analysis via XRD, microstructure observation via SEM and
bonding analysis via FTIR has revealed the existence of hydrosodalite phase in comparison with pure kao�lin and metakaolin. The result also indicated the lower NaOH (4 M) molarity gave a higher percentage of
hydrosodalite formation in comparison with higher molarity of NaOH at 5 M, 6 M and 7 M. |
first_indexed | 2024-03-05T21:54:24Z |
format | Article |
id | uthm.eprints-6644 |
institution | Universiti Tun Hussein Onn Malaysia |
language | English |
last_indexed | 2024-03-05T21:54:24Z |
publishDate | 2021 |
publisher | Elsevier |
record_format | dspace |
spelling | uthm.eprints-66442022-03-14T01:26:28Z http://eprints.uthm.edu.my/6644/ The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method Sazali, Norsuhailizah Harun, Zawati Azhar, Faiz Hafeez Bahri, Syamsutajri Syamsol Raja Ahmad, Raja Puteri Nurul Adibah Hussin@Isa, Rosniza Misdan, Nurasyikin TJ Mechanical engineering and machinery In this present work, hydrosodalite was successfully synthesized by hydrothermal method from the raw Johor kaolin, Malaysia. In order to get the size that was less than 63 lm, the raw kaolin was ground and sieved. Since the raw kaolin did not undergo the beneficiation process, thus the raw kaolin then was calcinated for four hours at 650 �C to produce more reactive clay (metakaolin). The synthesizing of hydrosodalite form of the metakaolin powder was conducted by mixing the powder with different molar�ities of sodium hydroxide, NaOH. This mixture was further treated by soaking it at a temperature of 40 �C for 24 h. The reaction mixture was then moved for 12 h into the autoclave for the 100 �C under hydrother�mal conditions. The results through phase analysis via XRD, microstructure observation via SEM and bonding analysis via FTIR has revealed the existence of hydrosodalite phase in comparison with pure kao�lin and metakaolin. The result also indicated the lower NaOH (4 M) molarity gave a higher percentage of hydrosodalite formation in comparison with higher molarity of NaOH at 5 M, 6 M and 7 M. Elsevier 2021 Article PeerReviewed text en http://eprints.uthm.edu.my/6644/1/P13067_f086c1fd022be8be32b84fad851d59e1.pdf Sazali, Norsuhailizah and Harun, Zawati and Azhar, Faiz Hafeez and Bahri, Syamsutajri Syamsol and Raja Ahmad, Raja Puteri Nurul Adibah and Hussin@Isa, Rosniza and Misdan, Nurasyikin (2021) The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method. Materials Today: Proceedings, 46. pp. 2045-2051. https://doi.org/10.1016/j.matpr.2021.03.135 |
spellingShingle | TJ Mechanical engineering and machinery Sazali, Norsuhailizah Harun, Zawati Azhar, Faiz Hafeez Bahri, Syamsutajri Syamsol Raja Ahmad, Raja Puteri Nurul Adibah Hussin@Isa, Rosniza Misdan, Nurasyikin The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method |
title | The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method |
title_full | The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method |
title_fullStr | The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method |
title_full_unstemmed | The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method |
title_short | The effect of various molarity sodium hydroxide (NaOH) on the hydrosodalite formation from synthesis of Johor Kaolin, Malaysia by hydrothermal method |
title_sort | effect of various molarity sodium hydroxide naoh on the hydrosodalite formation from synthesis of johor kaolin malaysia by hydrothermal method |
topic | TJ Mechanical engineering and machinery |
url | http://eprints.uthm.edu.my/6644/1/P13067_f086c1fd022be8be32b84fad851d59e1.pdf |
work_keys_str_mv | AT sazalinorsuhailizah theeffectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT harunzawati theeffectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT azharfaizhafeez theeffectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT bahrisyamsutajrisyamsol theeffectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT rajaahmadrajaputerinuruladibah theeffectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT hussinisarosniza theeffectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT misdannurasyikin theeffectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT sazalinorsuhailizah effectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT harunzawati effectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT azharfaizhafeez effectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT bahrisyamsutajrisyamsol effectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT rajaahmadrajaputerinuruladibah effectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT hussinisarosniza effectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod AT misdannurasyikin effectofvariousmolaritysodiumhydroxidenaohonthehydrosodaliteformationfromsynthesisofjohorkaolinmalaysiabyhydrothermalmethod |