Potential of transforming sodalite from synthesis kaolin with a mild condition of the hydrothermal method

The hydrothermal synthesis method is one of the successful methods for transforming kaolin into sodalite with various parameters considered. The variation of alkalinity source of 2-3 Molarity of sodium hydroxide and crystallization time (12-16 hours) was considered an important parameter that...

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Main Authors: Sazali, Norsuhailizah, Harun, Zawati, Abdullahi, Tijjani, Azhar, Faiz Hafeez, Ahmad, Azlinnorazia, Rasli, Nurul Izwanie, Sazali, Norazlianie
Format: Article
Language:English
Published: AMG Transcend Association 2022
Subjects:
Online Access:http://eprints.uthm.edu.my/6868/1/J13781_ce3501e7e88804535eb44cb52e9cc2df.pdf
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author Sazali, Norsuhailizah
Harun, Zawati
Abdullahi, Tijjani
Azhar, Faiz Hafeez
Ahmad, Azlinnorazia
Rasli, Nurul Izwanie
Sazali, Norazlianie
author_facet Sazali, Norsuhailizah
Harun, Zawati
Abdullahi, Tijjani
Azhar, Faiz Hafeez
Ahmad, Azlinnorazia
Rasli, Nurul Izwanie
Sazali, Norazlianie
author_sort Sazali, Norsuhailizah
collection UTHM
description The hydrothermal synthesis method is one of the successful methods for transforming kaolin into sodalite with various parameters considered. The variation of alkalinity source of 2-3 Molarity of sodium hydroxide and crystallization time (12-16 hours) was considered an important parameter that influences the formation of sodalite. It is reported in this research that the process of synthesizing sodalite to transform into an amorphous stage (Metakaolinization phase) began with beneficiation of kaolin to remove the impurities and calcination by 6500C for four hours. The synthesis was done through an aging process (400C, 24 hours), and the crystallization temperature was 1000C. The kaolin was characterized by XRD, FESEM, FTIR, PSA, TGA, followed with metakaolin by XRD, FESEM, FTIR, and the end-product by XRD, FESEM, FTIR, and PSA. The crystallinity percentage of sodalite slightly increased by increasing the molarity and crystallization time, but quartz remains in the end-product.
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spelling uthm.eprints-68682022-03-28T08:00:00Z http://eprints.uthm.edu.my/6868/ Potential of transforming sodalite from synthesis kaolin with a mild condition of the hydrothermal method Sazali, Norsuhailizah Harun, Zawati Abdullahi, Tijjani Azhar, Faiz Hafeez Ahmad, Azlinnorazia Rasli, Nurul Izwanie Sazali, Norazlianie TP Chemical technology The hydrothermal synthesis method is one of the successful methods for transforming kaolin into sodalite with various parameters considered. The variation of alkalinity source of 2-3 Molarity of sodium hydroxide and crystallization time (12-16 hours) was considered an important parameter that influences the formation of sodalite. It is reported in this research that the process of synthesizing sodalite to transform into an amorphous stage (Metakaolinization phase) began with beneficiation of kaolin to remove the impurities and calcination by 6500C for four hours. The synthesis was done through an aging process (400C, 24 hours), and the crystallization temperature was 1000C. The kaolin was characterized by XRD, FESEM, FTIR, PSA, TGA, followed with metakaolin by XRD, FESEM, FTIR, and the end-product by XRD, FESEM, FTIR, and PSA. The crystallinity percentage of sodalite slightly increased by increasing the molarity and crystallization time, but quartz remains in the end-product. AMG Transcend Association 2022 Article PeerReviewed text en http://eprints.uthm.edu.my/6868/1/J13781_ce3501e7e88804535eb44cb52e9cc2df.pdf Sazali, Norsuhailizah and Harun, Zawati and Abdullahi, Tijjani and Azhar, Faiz Hafeez and Ahmad, Azlinnorazia and Rasli, Nurul Izwanie and Sazali, Norazlianie (2022) Potential of transforming sodalite from synthesis kaolin with a mild condition of the hydrothermal method. Biointerface Research in Applied Chemistry, 12 (6). pp. 7376-7393. ISSN 2069-5837 https://doi.org/10.33263/BRIAC126.73767393
spellingShingle TP Chemical technology
Sazali, Norsuhailizah
Harun, Zawati
Abdullahi, Tijjani
Azhar, Faiz Hafeez
Ahmad, Azlinnorazia
Rasli, Nurul Izwanie
Sazali, Norazlianie
Potential of transforming sodalite from synthesis kaolin with a mild condition of the hydrothermal method
title Potential of transforming sodalite from synthesis kaolin with a mild condition of the hydrothermal method
title_full Potential of transforming sodalite from synthesis kaolin with a mild condition of the hydrothermal method
title_fullStr Potential of transforming sodalite from synthesis kaolin with a mild condition of the hydrothermal method
title_full_unstemmed Potential of transforming sodalite from synthesis kaolin with a mild condition of the hydrothermal method
title_short Potential of transforming sodalite from synthesis kaolin with a mild condition of the hydrothermal method
title_sort potential of transforming sodalite from synthesis kaolin with a mild condition of the hydrothermal method
topic TP Chemical technology
url http://eprints.uthm.edu.my/6868/1/J13781_ce3501e7e88804535eb44cb52e9cc2df.pdf
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