Time-resolved studies of the early hydration of cements using synchrotron energy-dispersive diffraction

We outline the need to study the early hydration of cements by dynamic diffraction methods, and demonstrate how this can be done using a “hydration cell” designed specifically for the parallel beam geometry of synchrotron energy-dispersive diffraction. The method has been applied to three systems: a...

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Main Authors: Paul B, Barnes, Clark, Simon Martin, Häusermann, Daniel, Henderson, Eric W., Fentiman, Charles H., Muhamad, Mohamed Noor, Rashid, Shahwana
Format: Article
Published: Taylor and Francis, Reading, ROYAUME-UNI (1979) (Revue) 1992
Subjects:
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author Paul B, Barnes
Clark, Simon Martin
Häusermann, Daniel
Henderson, Eric W.
Fentiman, Charles H.
Muhamad, Mohamed Noor
Rashid, Shahwana
author_facet Paul B, Barnes
Clark, Simon Martin
Häusermann, Daniel
Henderson, Eric W.
Fentiman, Charles H.
Muhamad, Mohamed Noor
Rashid, Shahwana
author_sort Paul B, Barnes
collection ePrints
description We outline the need to study the early hydration of cements by dynamic diffraction methods, and demonstrate how this can be done using a “hydration cell” designed specifically for the parallel beam geometry of synchrotron energy-dispersive diffraction. The method has been applied to three systems: a model component of portland cement, a high-alumina cement and an ettringite-based cement. The results show how this technique might be used to gather information on the kinetics of the chemical processes involved. In the case of ettringite, we can follow dynamically the crystallisation process on an unprecedented 20 second time scale. © 1992, Taylor & Francis Group, LLC. All rights reserved.
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spelling utm.eprints-25012017-10-23T08:17:01Z http://eprints.utm.my/2501/ Time-resolved studies of the early hydration of cements using synchrotron energy-dispersive diffraction Paul B, Barnes Clark, Simon Martin Häusermann, Daniel Henderson, Eric W. Fentiman, Charles H. Muhamad, Mohamed Noor Rashid, Shahwana Q Science (General) QD Chemistry QC Physics We outline the need to study the early hydration of cements by dynamic diffraction methods, and demonstrate how this can be done using a “hydration cell” designed specifically for the parallel beam geometry of synchrotron energy-dispersive diffraction. The method has been applied to three systems: a model component of portland cement, a high-alumina cement and an ettringite-based cement. The results show how this technique might be used to gather information on the kinetics of the chemical processes involved. In the case of ettringite, we can follow dynamically the crystallisation process on an unprecedented 20 second time scale. © 1992, Taylor & Francis Group, LLC. All rights reserved. Taylor and Francis, Reading, ROYAUME-UNI (1979) (Revue) 1992 Article PeerReviewed Paul B, Barnes and Clark, Simon Martin and Häusermann, Daniel and Henderson, Eric W. and Fentiman, Charles H. and Muhamad, Mohamed Noor and Rashid, Shahwana (1992) Time-resolved studies of the early hydration of cements using synchrotron energy-dispersive diffraction. Phase transitions , 39 . pp. 117-128. http://dx.doi.org/10.1080/01411599208203475
spellingShingle Q Science (General)
QD Chemistry
QC Physics
Paul B, Barnes
Clark, Simon Martin
Häusermann, Daniel
Henderson, Eric W.
Fentiman, Charles H.
Muhamad, Mohamed Noor
Rashid, Shahwana
Time-resolved studies of the early hydration of cements using synchrotron energy-dispersive diffraction
title Time-resolved studies of the early hydration of cements using synchrotron energy-dispersive diffraction
title_full Time-resolved studies of the early hydration of cements using synchrotron energy-dispersive diffraction
title_fullStr Time-resolved studies of the early hydration of cements using synchrotron energy-dispersive diffraction
title_full_unstemmed Time-resolved studies of the early hydration of cements using synchrotron energy-dispersive diffraction
title_short Time-resolved studies of the early hydration of cements using synchrotron energy-dispersive diffraction
title_sort time resolved studies of the early hydration of cements using synchrotron energy dispersive diffraction
topic Q Science (General)
QD Chemistry
QC Physics
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