Spectroscopic analysis of cis-polyisoprene and polymethyl methacrylate graft copolymers

This paper explains the used of Fourier Transform Infra-Red Spectroscopy (FTIR) Nocolet MX-1 in analysing the PMMA content of the graft copolymer cis-polyisoprene/PMMA leading to its suspected mechanism. Both qualitative and quantitative applications were used. Graft copolymers were synthesized b...

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Main Author: Wan Abdul Rahman, Wan Aizan
Format: Article
Language:English
Published: Faculty of Chemical & Natural Resources Engineering 1990
Subjects:
Online Access:http://eprints.utm.my/4540/1/WanAizan1990_SpectroscopicAnalysisOfCisPolyisoprene.pdf
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author Wan Abdul Rahman, Wan Aizan
author_facet Wan Abdul Rahman, Wan Aizan
author_sort Wan Abdul Rahman, Wan Aizan
collection ePrints
description This paper explains the used of Fourier Transform Infra-Red Spectroscopy (FTIR) Nocolet MX-1 in analysing the PMMA content of the graft copolymer cis-polyisoprene/PMMA leading to its suspected mechanism. Both qualitative and quantitative applications were used. Graft copolymers were synthesized by free-radical polymerization utililising benzoyl peroxide as an initiator and toluene as the solvent. Samples were analysed for three different polymerization time. The proposed grafting mechanism were confirmed by FTIR analysis on the product obtained after the degradation of the backbone chain. Calibration of the FTIR was accomplished with the used of PMMA standard of number average molecular weight, Mn 125, 000.
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spelling utm.eprints-45402017-10-16T01:23:00Z http://eprints.utm.my/4540/ Spectroscopic analysis of cis-polyisoprene and polymethyl methacrylate graft copolymers Wan Abdul Rahman, Wan Aizan T Technology (General) This paper explains the used of Fourier Transform Infra-Red Spectroscopy (FTIR) Nocolet MX-1 in analysing the PMMA content of the graft copolymer cis-polyisoprene/PMMA leading to its suspected mechanism. Both qualitative and quantitative applications were used. Graft copolymers were synthesized by free-radical polymerization utililising benzoyl peroxide as an initiator and toluene as the solvent. Samples were analysed for three different polymerization time. The proposed grafting mechanism were confirmed by FTIR analysis on the product obtained after the degradation of the backbone chain. Calibration of the FTIR was accomplished with the used of PMMA standard of number average molecular weight, Mn 125, 000. Faculty of Chemical & Natural Resources Engineering 1990-06 Article PeerReviewed application/pdf en http://eprints.utm.my/4540/1/WanAizan1990_SpectroscopicAnalysisOfCisPolyisoprene.pdf Wan Abdul Rahman, Wan Aizan (1990) Spectroscopic analysis of cis-polyisoprene and polymethyl methacrylate graft copolymers. Buletin FKKKSA, 4 (1). pp. 36-50. ISSN 0128-0740
spellingShingle T Technology (General)
Wan Abdul Rahman, Wan Aizan
Spectroscopic analysis of cis-polyisoprene and polymethyl methacrylate graft copolymers
title Spectroscopic analysis of cis-polyisoprene and polymethyl methacrylate graft copolymers
title_full Spectroscopic analysis of cis-polyisoprene and polymethyl methacrylate graft copolymers
title_fullStr Spectroscopic analysis of cis-polyisoprene and polymethyl methacrylate graft copolymers
title_full_unstemmed Spectroscopic analysis of cis-polyisoprene and polymethyl methacrylate graft copolymers
title_short Spectroscopic analysis of cis-polyisoprene and polymethyl methacrylate graft copolymers
title_sort spectroscopic analysis of cis polyisoprene and polymethyl methacrylate graft copolymers
topic T Technology (General)
url http://eprints.utm.my/4540/1/WanAizan1990_SpectroscopicAnalysisOfCisPolyisoprene.pdf
work_keys_str_mv AT wanabdulrahmanwanaizan spectroscopicanalysisofcispolyisopreneandpolymethylmethacrylategraftcopolymers