Fesem-edx and CV characteristics of dopant (mn, co, ni) magnesium ferrites

Doping magnesium ferrites (MgFe2 O4) with Mn, Co and Ni, which were synthesized by sol gel method using citric acid and polyvinyl alcohol (P VA) and calcined at 500oC, showed interesting electrochemical featur es based on their cyclic voltammetric (CV) characteristics using 5 µL ferrite – poly vinyl...

Full description

Bibliographic Details
Main Authors: Jonit, S. S., Aziz, M., Sundari, R.
Format: Conference or Workshop Item
Published: 2013
Subjects:
_version_ 1796859568905519104
author Jonit, S. S.
Aziz, M.
Sundari, R.
author_facet Jonit, S. S.
Aziz, M.
Sundari, R.
author_sort Jonit, S. S.
collection ePrints
description Doping magnesium ferrites (MgFe2 O4) with Mn, Co and Ni, which were synthesized by sol gel method using citric acid and polyvinyl alcohol (P VA) and calcined at 500oC, showed interesting electrochemical featur es based on their cyclic voltammetric (CV) characteristics using 5 µL ferrite – poly vinylidene fluoride in ethano l deposited on a screen printed carbon electrode (SPCE) in a mixture of 1.0 M KOH and ferricyanide solution recorded with a scan rate of 0.02 Vs -1. The Mn doped magnesium ferrite (x = 0.9) showed the most remarkable CV performance over other doped element (Co and Ni) and un-doped magnesiu m ferrites. The surface morphology of doped ferrites was studied by applying a field emissi on scanning electron microscope (FESEM) in conjunction with an energy dispersive X-ray spect roscopy (EDX) analysis. The results revealed that Mn posed the highest percentage on the surface ( ≈ 21.5 %), followed by Co (≈ 19.5%) and Ni ( ≈ 6.7%) with respect to x = 0.9 of M0.9Mg0.1Fe 2 O4 (M = Co, Mn and Ni) at 500oC calcination. The study showed the possibility of yielding semi conducting ferrites using own fabricated magnesium ferrite and its metal doping.
first_indexed 2024-03-05T19:29:06Z
format Conference or Workshop Item
id utm.eprints-51070
institution Universiti Teknologi Malaysia - ePrints
last_indexed 2024-03-05T19:29:06Z
publishDate 2013
record_format dspace
spelling utm.eprints-510702017-09-17T06:33:29Z http://eprints.utm.my/51070/ Fesem-edx and CV characteristics of dopant (mn, co, ni) magnesium ferrites Jonit, S. S. Aziz, M. Sundari, R. Q Science Doping magnesium ferrites (MgFe2 O4) with Mn, Co and Ni, which were synthesized by sol gel method using citric acid and polyvinyl alcohol (P VA) and calcined at 500oC, showed interesting electrochemical featur es based on their cyclic voltammetric (CV) characteristics using 5 µL ferrite – poly vinylidene fluoride in ethano l deposited on a screen printed carbon electrode (SPCE) in a mixture of 1.0 M KOH and ferricyanide solution recorded with a scan rate of 0.02 Vs -1. The Mn doped magnesium ferrite (x = 0.9) showed the most remarkable CV performance over other doped element (Co and Ni) and un-doped magnesiu m ferrites. The surface morphology of doped ferrites was studied by applying a field emissi on scanning electron microscope (FESEM) in conjunction with an energy dispersive X-ray spect roscopy (EDX) analysis. The results revealed that Mn posed the highest percentage on the surface ( ≈ 21.5 %), followed by Co (≈ 19.5%) and Ni ( ≈ 6.7%) with respect to x = 0.9 of M0.9Mg0.1Fe 2 O4 (M = Co, Mn and Ni) at 500oC calcination. The study showed the possibility of yielding semi conducting ferrites using own fabricated magnesium ferrite and its metal doping. 2013 Conference or Workshop Item PeerReviewed Jonit, S. S. and Aziz, M. and Sundari, R. (2013) Fesem-edx and CV characteristics of dopant (mn, co, ni) magnesium ferrites. In: Advanced Materials Research. http://dx.doi.org/10.4028/www.scientific.net/AMR.645.150
spellingShingle Q Science
Jonit, S. S.
Aziz, M.
Sundari, R.
Fesem-edx and CV characteristics of dopant (mn, co, ni) magnesium ferrites
title Fesem-edx and CV characteristics of dopant (mn, co, ni) magnesium ferrites
title_full Fesem-edx and CV characteristics of dopant (mn, co, ni) magnesium ferrites
title_fullStr Fesem-edx and CV characteristics of dopant (mn, co, ni) magnesium ferrites
title_full_unstemmed Fesem-edx and CV characteristics of dopant (mn, co, ni) magnesium ferrites
title_short Fesem-edx and CV characteristics of dopant (mn, co, ni) magnesium ferrites
title_sort fesem edx and cv characteristics of dopant mn co ni magnesium ferrites
topic Q Science
work_keys_str_mv AT jonitss fesemedxandcvcharacteristicsofdopantmnconimagnesiumferrites
AT azizm fesemedxandcvcharacteristicsofdopantmnconimagnesiumferrites
AT sundarir fesemedxandcvcharacteristicsofdopantmnconimagnesiumferrites