Influence of thermal treatment on microstructure, mechanical and degradation properties of Zn-3Mg alloy as potential biodegradable implant material

In this study, the influence of homogenisation heat treatment effect on Zn-3Mg alloy proposed for biodegradable bone implants was investigated. The alloy was developed via casting process from high purity raw materials and homogenised at 360°C for 15h followed by water quenching. Results revealed th...

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Main Authors: Dambatta, M. S., Sudin, Izman, Kurniawan, Denni, Saeed, Farahany, Yahaya, Bashir, Hermawan, Hendra
Format: Article
Published: Elsevier 2015
Subjects:
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author Dambatta, M. S.
Sudin, Izman
Kurniawan, Denni
Saeed, Farahany
Yahaya, Bashir
Hermawan, Hendra
author_facet Dambatta, M. S.
Sudin, Izman
Kurniawan, Denni
Saeed, Farahany
Yahaya, Bashir
Hermawan, Hendra
author_sort Dambatta, M. S.
collection ePrints
description In this study, the influence of homogenisation heat treatment effect on Zn-3Mg alloy proposed for biodegradable bone implants was investigated. The alloy was developed via casting process from high purity raw materials and homogenised at 360°C for 15h followed by water quenching. Results revealed that the microstructure of as cast alloy was composed of dendritic structure of Zn-rich phase distributed in segregated pattern within Mg2Zn11 eutectic phase. Exposure to the long duration heating of homogenisation apparently broke the dendrites and transformed them into connected precipitates within the alloy's matrix. Non-equilibrium thermal analysis revealed the formation of Mg2Zn11 eutectic phase which nucleated at 367°C and solidified completely at 354°C. The eutectic coherency point occurred at 368°C and 424s when 30% of solid has precipitated during solidification. Homogenisation resulted into lowering the alloy's tensile strength from 104MPa to 88MPa but improving elongation at fracture from 2.3% to 8.8%. The homogenised Zn-3Mg alloy showed improved corrosion resistance (corrosion rate=0.13mmpy) compared to the as-cast one (corrosion rate=0.21mmpy). The mechanical property and corrosion behaviour of the homogenised alloy seem suitable for biodegradable implant applications
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spelling utm.eprints-559342017-08-25T08:54:33Z http://eprints.utm.my/55934/ Influence of thermal treatment on microstructure, mechanical and degradation properties of Zn-3Mg alloy as potential biodegradable implant material Dambatta, M. S. Sudin, Izman Kurniawan, Denni Saeed, Farahany Yahaya, Bashir Hermawan, Hendra TJ Mechanical engineering and machinery In this study, the influence of homogenisation heat treatment effect on Zn-3Mg alloy proposed for biodegradable bone implants was investigated. The alloy was developed via casting process from high purity raw materials and homogenised at 360°C for 15h followed by water quenching. Results revealed that the microstructure of as cast alloy was composed of dendritic structure of Zn-rich phase distributed in segregated pattern within Mg2Zn11 eutectic phase. Exposure to the long duration heating of homogenisation apparently broke the dendrites and transformed them into connected precipitates within the alloy's matrix. Non-equilibrium thermal analysis revealed the formation of Mg2Zn11 eutectic phase which nucleated at 367°C and solidified completely at 354°C. The eutectic coherency point occurred at 368°C and 424s when 30% of solid has precipitated during solidification. Homogenisation resulted into lowering the alloy's tensile strength from 104MPa to 88MPa but improving elongation at fracture from 2.3% to 8.8%. The homogenised Zn-3Mg alloy showed improved corrosion resistance (corrosion rate=0.13mmpy) compared to the as-cast one (corrosion rate=0.21mmpy). The mechanical property and corrosion behaviour of the homogenised alloy seem suitable for biodegradable implant applications Elsevier 2015-11 Article PeerReviewed Dambatta, M. S. and Sudin, Izman and Kurniawan, Denni and Saeed, Farahany and Yahaya, Bashir and Hermawan, Hendra (2015) Influence of thermal treatment on microstructure, mechanical and degradation properties of Zn-3Mg alloy as potential biodegradable implant material. Materials and Design, 85 . pp. 431-437. ISSN 0264-1275 http://dx.doi.org/10.1016/j.matdes.2015.06.181 DOI:10.1016/j.matdes.2015.06.181
spellingShingle TJ Mechanical engineering and machinery
Dambatta, M. S.
Sudin, Izman
Kurniawan, Denni
Saeed, Farahany
Yahaya, Bashir
Hermawan, Hendra
Influence of thermal treatment on microstructure, mechanical and degradation properties of Zn-3Mg alloy as potential biodegradable implant material
title Influence of thermal treatment on microstructure, mechanical and degradation properties of Zn-3Mg alloy as potential biodegradable implant material
title_full Influence of thermal treatment on microstructure, mechanical and degradation properties of Zn-3Mg alloy as potential biodegradable implant material
title_fullStr Influence of thermal treatment on microstructure, mechanical and degradation properties of Zn-3Mg alloy as potential biodegradable implant material
title_full_unstemmed Influence of thermal treatment on microstructure, mechanical and degradation properties of Zn-3Mg alloy as potential biodegradable implant material
title_short Influence of thermal treatment on microstructure, mechanical and degradation properties of Zn-3Mg alloy as potential biodegradable implant material
title_sort influence of thermal treatment on microstructure mechanical and degradation properties of zn 3mg alloy as potential biodegradable implant material
topic TJ Mechanical engineering and machinery
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