Rapid systhesis of graphene nanosheets and its structural properties study for direct methanol fuel cell

Titanium dioxide nanofibers with diameter ranging to several nanometers were synthesized via electrospinning technique. The precursor solution was prepared by mixing the polyvinylpyrrolidone, PVP (MW-l,300,OOO) in ethanol, meanwhile titanium tetraisopropoxide, TTIP in acetic acid was slowly added in...

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Main Authors: Mohamad Nor, Nor Azureen, Jaafar, Juhana, Ismail, Ahmad Fauzi, Othman, Mohd. Hafiz Dzarfan, Rahman, Mukhlis A., Wan Salleh, Wan Norharyati, Yusof, Norhaniza, Lau, Woei Jye
Format: Conference or Workshop Item
Published: 2015
Subjects:
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author Mohamad Nor, Nor Azureen
Jaafar, Juhana
Ismail, Ahmad Fauzi
Othman, Mohd. Hafiz Dzarfan
Rahman, Mukhlis A.
Wan Salleh, Wan Norharyati
Yusof, Norhaniza
Lau, Woei Jye
author_facet Mohamad Nor, Nor Azureen
Jaafar, Juhana
Ismail, Ahmad Fauzi
Othman, Mohd. Hafiz Dzarfan
Rahman, Mukhlis A.
Wan Salleh, Wan Norharyati
Yusof, Norhaniza
Lau, Woei Jye
author_sort Mohamad Nor, Nor Azureen
collection ePrints
description Titanium dioxide nanofibers with diameter ranging to several nanometers were synthesized via electrospinning technique. The precursor solution was prepared by mixing the polyvinylpyrrolidone, PVP (MW-l,300,OOO) in ethanol, meanwhile titanium tetraisopropoxide, TTIP in acetic acid was slowly added into the solution under a vigorous stirring. The precursor solutions were then used in the electrospinning process under high voltage supply. As-spun nanofibers were heatted. under different temperature 400°C, 500°C and 600°C. The TiO2 nanofibers were characterized by using ,scanning electron microscopy (SEM), Brunauer Emmett-Teller (BET) and X-raY .diffraction (XRD). The results indicated that the heat treated Ti02 nanofibers consist of anatase and rutile phases. As the calcination temperature increased (400-500C), the anatase phase are greater than rutile phase and specific surface area are decreases while the calcination process influenced the nanofibers diameter.
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spelling utm.eprints-617722017-04-26T06:28:33Z http://eprints.utm.my/61772/ Rapid systhesis of graphene nanosheets and its structural properties study for direct methanol fuel cell Mohamad Nor, Nor Azureen Jaafar, Juhana Ismail, Ahmad Fauzi Othman, Mohd. Hafiz Dzarfan Rahman, Mukhlis A. Wan Salleh, Wan Norharyati Yusof, Norhaniza Lau, Woei Jye TP Chemical technology Titanium dioxide nanofibers with diameter ranging to several nanometers were synthesized via electrospinning technique. The precursor solution was prepared by mixing the polyvinylpyrrolidone, PVP (MW-l,300,OOO) in ethanol, meanwhile titanium tetraisopropoxide, TTIP in acetic acid was slowly added into the solution under a vigorous stirring. The precursor solutions were then used in the electrospinning process under high voltage supply. As-spun nanofibers were heatted. under different temperature 400°C, 500°C and 600°C. The TiO2 nanofibers were characterized by using ,scanning electron microscopy (SEM), Brunauer Emmett-Teller (BET) and X-raY .diffraction (XRD). The results indicated that the heat treated Ti02 nanofibers consist of anatase and rutile phases. As the calcination temperature increased (400-500C), the anatase phase are greater than rutile phase and specific surface area are decreases while the calcination process influenced the nanofibers diameter. 2015 Conference or Workshop Item PeerReviewed Mohamad Nor, Nor Azureen and Jaafar, Juhana and Ismail, Ahmad Fauzi and Othman, Mohd. Hafiz Dzarfan and Rahman, Mukhlis A. and Wan Salleh, Wan Norharyati and Yusof, Norhaniza and Lau, Woei Jye (2015) Rapid systhesis of graphene nanosheets and its structural properties study for direct methanol fuel cell. In: The 4th ICIBA 2015, International Conference on Information Technology and Business Applications, 20-21 Feb, 2015, Indonesia. http://www.allconferencealerts.com/conference_details.php?eid=18338
spellingShingle TP Chemical technology
Mohamad Nor, Nor Azureen
Jaafar, Juhana
Ismail, Ahmad Fauzi
Othman, Mohd. Hafiz Dzarfan
Rahman, Mukhlis A.
Wan Salleh, Wan Norharyati
Yusof, Norhaniza
Lau, Woei Jye
Rapid systhesis of graphene nanosheets and its structural properties study for direct methanol fuel cell
title Rapid systhesis of graphene nanosheets and its structural properties study for direct methanol fuel cell
title_full Rapid systhesis of graphene nanosheets and its structural properties study for direct methanol fuel cell
title_fullStr Rapid systhesis of graphene nanosheets and its structural properties study for direct methanol fuel cell
title_full_unstemmed Rapid systhesis of graphene nanosheets and its structural properties study for direct methanol fuel cell
title_short Rapid systhesis of graphene nanosheets and its structural properties study for direct methanol fuel cell
title_sort rapid systhesis of graphene nanosheets and its structural properties study for direct methanol fuel cell
topic TP Chemical technology
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