Facile synthesis of nanorized zinc oxide by electrochemical method
Nanosized highly reactive zinc oxide (EGZnO/Naph) was readily synthesized by electrolysis of a N,Ndimethylformamide (DMF) solution containing naphthalene as a mediator followed by calcination at 823 K. XRD results showed that the product is high purity of zinc oxide. The particles size of EGZnO/Naph...
| Main Authors: | , , , , |
|---|---|
| Format: | Conference or Workshop Item |
| Published: |
2008
|
| Subjects: |
| _version_ | 1825909864081129472 |
|---|---|
| author | Musthofa, M. Razali, N. A. M. Hairon, N. H. Jalil, A. A. Trihwayono, S. |
| author_facet | Musthofa, M. Razali, N. A. M. Hairon, N. H. Jalil, A. A. Trihwayono, S. |
| author_sort | Musthofa, M. |
| collection | ePrints |
| description | Nanosized highly reactive zinc oxide (EGZnO/Naph) was readily synthesized by electrolysis of a N,Ndimethylformamide (DMF) solution containing naphthalene as a mediator followed by calcination at 823 K. XRD results showed that the product is high purity of zinc oxide. The particles size of EGZnO/Naph was confirmed by TEM which was varied between 10 to 30 nm. Nitrogen physisorption analysis showed that the surface area was 45.85 m2/g, which is 10 times larger than commercial zinc oxide. The FTIR spectrum shows the standard peak of zinc oxide at 450 cm−1. |
| first_indexed | 2024-03-05T18:08:29Z |
| format | Conference or Workshop Item |
| id | utm.eprints-6234 |
| institution | Universiti Teknologi Malaysia - ePrints |
| last_indexed | 2024-03-05T18:08:29Z |
| publishDate | 2008 |
| record_format | dspace |
| spelling | utm.eprints-62342017-09-07T03:42:57Z http://eprints.utm.my/6234/ Facile synthesis of nanorized zinc oxide by electrochemical method Musthofa, M. Razali, N. A. M. Hairon, N. H. Jalil, A. A. Trihwayono, S. QD Chemistry Nanosized highly reactive zinc oxide (EGZnO/Naph) was readily synthesized by electrolysis of a N,Ndimethylformamide (DMF) solution containing naphthalene as a mediator followed by calcination at 823 K. XRD results showed that the product is high purity of zinc oxide. The particles size of EGZnO/Naph was confirmed by TEM which was varied between 10 to 30 nm. Nitrogen physisorption analysis showed that the surface area was 45.85 m2/g, which is 10 times larger than commercial zinc oxide. The FTIR spectrum shows the standard peak of zinc oxide at 450 cm−1. 2008 Conference or Workshop Item PeerReviewed Musthofa, M. and Razali, N. A. M. and Hairon, N. H. and Jalil, A. A. and Trihwayono, S. (2008) Facile synthesis of nanorized zinc oxide by electrochemical method. In: Regional Annual Fundamental Science Seminar 2008 (RAFSS 2008), 27 - 29 May 2008, Ibnu Sina Institute for Fundamental Science Studies. |
| spellingShingle | QD Chemistry Musthofa, M. Razali, N. A. M. Hairon, N. H. Jalil, A. A. Trihwayono, S. Facile synthesis of nanorized zinc oxide by electrochemical method |
| title | Facile synthesis of nanorized zinc oxide by electrochemical method |
| title_full | Facile synthesis of nanorized zinc oxide by electrochemical method |
| title_fullStr | Facile synthesis of nanorized zinc oxide by electrochemical method |
| title_full_unstemmed | Facile synthesis of nanorized zinc oxide by electrochemical method |
| title_short | Facile synthesis of nanorized zinc oxide by electrochemical method |
| title_sort | facile synthesis of nanorized zinc oxide by electrochemical method |
| topic | QD Chemistry |
| work_keys_str_mv | AT musthofam facilesynthesisofnanorizedzincoxidebyelectrochemicalmethod AT razalinam facilesynthesisofnanorizedzincoxidebyelectrochemicalmethod AT haironnh facilesynthesisofnanorizedzincoxidebyelectrochemicalmethod AT jalilaa facilesynthesisofnanorizedzincoxidebyelectrochemicalmethod AT trihwayonos facilesynthesisofnanorizedzincoxidebyelectrochemicalmethod |