Synthesis and characterization of hybrid matrix with encapsulated organic sensing dyes for pH sensing application

Films of multi-organic indicators, encapsulated in silica-titania hybrid matrix with CTAB, have been synthesized using sol-gel dip coating method. Two types of stable,dense and uniform matrices were annealed at a 150 degrees C within two time intervals 1 h and 2 h by using 0.1 M and 0.5 M indicator...

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Main Authors: Islam, Shumaila, Abdul Rahman, Rosly, Othaman, Zulkafli, Riaz, Saira, Naseem, Shahzad
Format: Article
Published: Elsevier 2014
Subjects:
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author Islam, Shumaila
Abdul Rahman, Rosly
Othaman, Zulkafli
Riaz, Saira
Naseem, Shahzad
author_facet Islam, Shumaila
Abdul Rahman, Rosly
Othaman, Zulkafli
Riaz, Saira
Naseem, Shahzad
author_sort Islam, Shumaila
collection ePrints
description Films of multi-organic indicators, encapsulated in silica-titania hybrid matrix with CTAB, have been synthesized using sol-gel dip coating method. Two types of stable,dense and uniform matrices were annealed at a 150 degrees C within two time intervals 1 h and 2 h by using 0.1 M and 0.5 M indicator concentrations. Nanoparticles are uniformly distributed with size in the range from 15-28 nm. Matrices have high surface area (418.18-441.30 m(2)/g), which has more capability to sense the broader pH range. Spectroscopic studies showed the establishment of heterogeneous chemical bonding which indicative of stability of matrices with 69% porosity. The response of the sensor is optimum at pH 9. (C) 2014 The Korean Society of Industrial and Engineering Chemistry.
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spelling utm.eprints-627712017-06-14T00:33:13Z http://eprints.utm.my/62771/ Synthesis and characterization of hybrid matrix with encapsulated organic sensing dyes for pH sensing application Islam, Shumaila Abdul Rahman, Rosly Othaman, Zulkafli Riaz, Saira Naseem, Shahzad Q Science Films of multi-organic indicators, encapsulated in silica-titania hybrid matrix with CTAB, have been synthesized using sol-gel dip coating method. Two types of stable,dense and uniform matrices were annealed at a 150 degrees C within two time intervals 1 h and 2 h by using 0.1 M and 0.5 M indicator concentrations. Nanoparticles are uniformly distributed with size in the range from 15-28 nm. Matrices have high surface area (418.18-441.30 m(2)/g), which has more capability to sense the broader pH range. Spectroscopic studies showed the establishment of heterogeneous chemical bonding which indicative of stability of matrices with 69% porosity. The response of the sensor is optimum at pH 9. (C) 2014 The Korean Society of Industrial and Engineering Chemistry. Elsevier 2014 Article PeerReviewed Islam, Shumaila and Abdul Rahman, Rosly and Othaman, Zulkafli and Riaz, Saira and Naseem, Shahzad (2014) Synthesis and characterization of hybrid matrix with encapsulated organic sensing dyes for pH sensing application. Journal of Industrial and Engineering Chemistry, 20 (6). p. 4414. ISSN 1226-086X https://doi.org/10.1016/j.jiec.2014.02.008 DOI:10.1016/j.jiec.2014.02.008
spellingShingle Q Science
Islam, Shumaila
Abdul Rahman, Rosly
Othaman, Zulkafli
Riaz, Saira
Naseem, Shahzad
Synthesis and characterization of hybrid matrix with encapsulated organic sensing dyes for pH sensing application
title Synthesis and characterization of hybrid matrix with encapsulated organic sensing dyes for pH sensing application
title_full Synthesis and characterization of hybrid matrix with encapsulated organic sensing dyes for pH sensing application
title_fullStr Synthesis and characterization of hybrid matrix with encapsulated organic sensing dyes for pH sensing application
title_full_unstemmed Synthesis and characterization of hybrid matrix with encapsulated organic sensing dyes for pH sensing application
title_short Synthesis and characterization of hybrid matrix with encapsulated organic sensing dyes for pH sensing application
title_sort synthesis and characterization of hybrid matrix with encapsulated organic sensing dyes for ph sensing application
topic Q Science
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AT abdulrahmanrosly synthesisandcharacterizationofhybridmatrixwithencapsulatedorganicsensingdyesforphsensingapplication
AT othamanzulkafli synthesisandcharacterizationofhybridmatrixwithencapsulatedorganicsensingdyesforphsensingapplication
AT riazsaira synthesisandcharacterizationofhybridmatrixwithencapsulatedorganicsensingdyesforphsensingapplication
AT naseemshahzad synthesisandcharacterizationofhybridmatrixwithencapsulatedorganicsensingdyesforphsensingapplication