Thermal and tensile properties of poly(3- hydroxybutyrate)/ sepiolite nanocomposites
Sepiolite treated using microwave and chemical technique were obtained and compounded with poly(3-hydroxybutyrate) (PHB). The effect of reaction times exposing to the microwave rays was studied and characterized through multipychonometer and scanning electron microscopy (SEM). 12 minutes was found t...
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2015
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author | Ramli, Siti Aishah Adam, Safirah Othman, Norhayani |
author_facet | Ramli, Siti Aishah Adam, Safirah Othman, Norhayani |
author_sort | Ramli, Siti Aishah |
collection | ePrints |
description | Sepiolite treated using microwave and chemical technique were obtained and compounded with poly(3-hydroxybutyrate) (PHB). The effect of reaction times exposing to the microwave rays was studied and characterized through multipychonometer and scanning electron microscopy (SEM). 12 minutes was found to be the optimum reaction time in the microwave. Nanocomposites of PHB with different sepiolite loading (2, 4, 6, 8 and 10 wt %) were prepared using melt mixing. The thermal properties of the PHB nanocommposites were characterized through Differential Scanning Calorimeter (DSC) and Thermogravimetric Analysis (TGA). Addition of 2 wt% sepiolite into PHB increased the melting temperature and percent crystallinity of pure PHB. The crystallinity and melting temperature of PHB nanocomposites increased until 4 wt% loading and remained constant beyond 4 wt% sepiolite. Thermal stability of the nanocomposites slightly improved in the presence of sepiolite. Addition of sepiolite into PHB improved the tensile strength of pure PHB. |
first_indexed | 2024-03-05T19:56:46Z |
format | Conference or Workshop Item |
id | utm.eprints-63455 |
institution | Universiti Teknologi Malaysia - ePrints |
last_indexed | 2024-03-05T19:56:46Z |
publishDate | 2015 |
record_format | dspace |
spelling | utm.eprints-634552017-05-30T03:52:05Z http://eprints.utm.my/63455/ Thermal and tensile properties of poly(3- hydroxybutyrate)/ sepiolite nanocomposites Ramli, Siti Aishah Adam, Safirah Othman, Norhayani TP Chemical technology Sepiolite treated using microwave and chemical technique were obtained and compounded with poly(3-hydroxybutyrate) (PHB). The effect of reaction times exposing to the microwave rays was studied and characterized through multipychonometer and scanning electron microscopy (SEM). 12 minutes was found to be the optimum reaction time in the microwave. Nanocomposites of PHB with different sepiolite loading (2, 4, 6, 8 and 10 wt %) were prepared using melt mixing. The thermal properties of the PHB nanocommposites were characterized through Differential Scanning Calorimeter (DSC) and Thermogravimetric Analysis (TGA). Addition of 2 wt% sepiolite into PHB increased the melting temperature and percent crystallinity of pure PHB. The crystallinity and melting temperature of PHB nanocomposites increased until 4 wt% loading and remained constant beyond 4 wt% sepiolite. Thermal stability of the nanocomposites slightly improved in the presence of sepiolite. Addition of sepiolite into PHB improved the tensile strength of pure PHB. 2015 Conference or Workshop Item PeerReviewed Ramli, Siti Aishah and Adam, Safirah and Othman, Norhayani (2015) Thermal and tensile properties of poly(3- hydroxybutyrate)/ sepiolite nanocomposites. In: Malaysia Polymer International Conference (MPIC2015), 10-11 June, 2015, Kuala Lumpur, Malaysia. https://conferencealerts.com/show-event?id=146980 |
spellingShingle | TP Chemical technology Ramli, Siti Aishah Adam, Safirah Othman, Norhayani Thermal and tensile properties of poly(3- hydroxybutyrate)/ sepiolite nanocomposites |
title | Thermal and tensile properties of poly(3- hydroxybutyrate)/ sepiolite nanocomposites |
title_full | Thermal and tensile properties of poly(3- hydroxybutyrate)/ sepiolite nanocomposites |
title_fullStr | Thermal and tensile properties of poly(3- hydroxybutyrate)/ sepiolite nanocomposites |
title_full_unstemmed | Thermal and tensile properties of poly(3- hydroxybutyrate)/ sepiolite nanocomposites |
title_short | Thermal and tensile properties of poly(3- hydroxybutyrate)/ sepiolite nanocomposites |
title_sort | thermal and tensile properties of poly 3 hydroxybutyrate sepiolite nanocomposites |
topic | TP Chemical technology |
work_keys_str_mv | AT ramlisitiaishah thermalandtensilepropertiesofpoly3hydroxybutyratesepiolitenanocomposites AT adamsafirah thermalandtensilepropertiesofpoly3hydroxybutyratesepiolitenanocomposites AT othmannorhayani thermalandtensilepropertiesofpoly3hydroxybutyratesepiolitenanocomposites |