Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization

A series of nitrogen doped titania nanomaterials were synthesized via sol-gel method by using tetraethyl ammonium hydroxide as N source. Doping of N into TiO2 was confirmed via X-ray diffraction (XRD) and fourier transform infrared spectroscopy (FTIR) analyses. Mixture of anatase and rutile phases a...

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Main Authors: Zainal, N. D., Nur, H., Ling Lee, S.
Format: Article
Language:English
Published: Penerbit UTM Press 2016
Subjects:
Online Access:http://eprints.utm.my/74347/1/NurulDiyanaZainal2016_HighlyHomogeneousNitrogenDopedTitania.pdf
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author Zainal, N. D.
Nur, H.
Ling Lee, S.
author_facet Zainal, N. D.
Nur, H.
Ling Lee, S.
author_sort Zainal, N. D.
collection ePrints
description A series of nitrogen doped titania nanomaterials were synthesized via sol-gel method by using tetraethyl ammonium hydroxide as N source. Doping of N into TiO2 was confirmed via X-ray diffraction (XRD) and fourier transform infrared spectroscopy (FTIR) analyses. Mixture of anatase and rutile phases appeared in the unmodified TiO2 which was calcined at 773 K. The addition of N to TiO2 matrix led to formation of single phase of anatase. It has been demonstrated that TiO2 and all the N-doped TiO2 materials were in nanoscale ranging 15.91 – 20.82 nm. Change in surface morphology after N doping was detected by field emission scanning electron microscope (FESEM). Results of EDX mapping analysis indicated homogeneous distribution of N dopants.
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spelling utm.eprints-743472017-11-22T12:07:41Z http://eprints.utm.my/74347/ Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization Zainal, N. D. Nur, H. Ling Lee, S. QD Chemistry A series of nitrogen doped titania nanomaterials were synthesized via sol-gel method by using tetraethyl ammonium hydroxide as N source. Doping of N into TiO2 was confirmed via X-ray diffraction (XRD) and fourier transform infrared spectroscopy (FTIR) analyses. Mixture of anatase and rutile phases appeared in the unmodified TiO2 which was calcined at 773 K. The addition of N to TiO2 matrix led to formation of single phase of anatase. It has been demonstrated that TiO2 and all the N-doped TiO2 materials were in nanoscale ranging 15.91 – 20.82 nm. Change in surface morphology after N doping was detected by field emission scanning electron microscope (FESEM). Results of EDX mapping analysis indicated homogeneous distribution of N dopants. Penerbit UTM Press 2016 Article PeerReviewed application/pdf en http://eprints.utm.my/74347/1/NurulDiyanaZainal2016_HighlyHomogeneousNitrogenDopedTitania.pdf Zainal, N. D. and Nur, H. and Ling Lee, S. (2016) Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization. Jurnal Teknologi, 78 (6-12). pp. 117-120. ISSN 0127-9696 https://www.scopus.com/inward/record.uri?eid=2-s2.0-84976513504&doi=10.11113%2fjt.v78.9241&partnerID=40&md5=f58d53ff70133651d2eba1256f647401
spellingShingle QD Chemistry
Zainal, N. D.
Nur, H.
Ling Lee, S.
Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization
title Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization
title_full Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization
title_fullStr Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization
title_full_unstemmed Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization
title_short Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization
title_sort highly homogeneous nitrogen doped titania nanomaterials synthesis and characterization
topic QD Chemistry
url http://eprints.utm.my/74347/1/NurulDiyanaZainal2016_HighlyHomogeneousNitrogenDopedTitania.pdf
work_keys_str_mv AT zainalnd highlyhomogeneousnitrogendopedtitaniananomaterialssynthesisandcharacterization
AT nurh highlyhomogeneousnitrogendopedtitaniananomaterialssynthesisandcharacterization
AT linglees highlyhomogeneousnitrogendopedtitaniananomaterialssynthesisandcharacterization