Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization
A series of nitrogen doped titania nanomaterials were synthesized via sol-gel method by using tetraethyl ammonium hydroxide as N source. Doping of N into TiO2 was confirmed via X-ray diffraction (XRD) and fourier transform infrared spectroscopy (FTIR) analyses. Mixture of anatase and rutile phases a...
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Penerbit UTM Press
2016
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Online Access: | http://eprints.utm.my/74347/1/NurulDiyanaZainal2016_HighlyHomogeneousNitrogenDopedTitania.pdf |
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author | Zainal, N. D. Nur, H. Ling Lee, S. |
author_facet | Zainal, N. D. Nur, H. Ling Lee, S. |
author_sort | Zainal, N. D. |
collection | ePrints |
description | A series of nitrogen doped titania nanomaterials were synthesized via sol-gel method by using tetraethyl ammonium hydroxide as N source. Doping of N into TiO2 was confirmed via X-ray diffraction (XRD) and fourier transform infrared spectroscopy (FTIR) analyses. Mixture of anatase and rutile phases appeared in the unmodified TiO2 which was calcined at 773 K. The addition of N to TiO2 matrix led to formation of single phase of anatase. It has been demonstrated that TiO2 and all the N-doped TiO2 materials were in nanoscale ranging 15.91 – 20.82 nm. Change in surface morphology after N doping was detected by field emission scanning electron microscope (FESEM). Results of EDX mapping analysis indicated homogeneous distribution of N dopants. |
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format | Article |
id | utm.eprints-74347 |
institution | Universiti Teknologi Malaysia - ePrints |
language | English |
last_indexed | 2024-03-05T20:07:54Z |
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spelling | utm.eprints-743472017-11-22T12:07:41Z http://eprints.utm.my/74347/ Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization Zainal, N. D. Nur, H. Ling Lee, S. QD Chemistry A series of nitrogen doped titania nanomaterials were synthesized via sol-gel method by using tetraethyl ammonium hydroxide as N source. Doping of N into TiO2 was confirmed via X-ray diffraction (XRD) and fourier transform infrared spectroscopy (FTIR) analyses. Mixture of anatase and rutile phases appeared in the unmodified TiO2 which was calcined at 773 K. The addition of N to TiO2 matrix led to formation of single phase of anatase. It has been demonstrated that TiO2 and all the N-doped TiO2 materials were in nanoscale ranging 15.91 – 20.82 nm. Change in surface morphology after N doping was detected by field emission scanning electron microscope (FESEM). Results of EDX mapping analysis indicated homogeneous distribution of N dopants. Penerbit UTM Press 2016 Article PeerReviewed application/pdf en http://eprints.utm.my/74347/1/NurulDiyanaZainal2016_HighlyHomogeneousNitrogenDopedTitania.pdf Zainal, N. D. and Nur, H. and Ling Lee, S. (2016) Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization. Jurnal Teknologi, 78 (6-12). pp. 117-120. ISSN 0127-9696 https://www.scopus.com/inward/record.uri?eid=2-s2.0-84976513504&doi=10.11113%2fjt.v78.9241&partnerID=40&md5=f58d53ff70133651d2eba1256f647401 |
spellingShingle | QD Chemistry Zainal, N. D. Nur, H. Ling Lee, S. Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization |
title | Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization |
title_full | Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization |
title_fullStr | Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization |
title_full_unstemmed | Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization |
title_short | Highly homogeneous nitrogen doped titania nanomaterials: Synthesis and characterization |
title_sort | highly homogeneous nitrogen doped titania nanomaterials synthesis and characterization |
topic | QD Chemistry |
url | http://eprints.utm.my/74347/1/NurulDiyanaZainal2016_HighlyHomogeneousNitrogenDopedTitania.pdf |
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