Optimization of chemical pretreatment for removing cobalt on tungsten carbide substrate using response surface methodology

Diamond coating are commonly used in industries especially for application such as cutting tools, biomedical components, optical lenses, microelectronics, engineering, and thermal management systems. The diamond coating quality is strongly depending on substrate preparation prior to diamond coating....

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Main Authors: Shah, A., Izman, S., Hassan, M. A., Mustapha, R.
Format: Article
Language:English
Published: Penerbit UTM Press 2016
Subjects:
Online Access:http://eprints.utm.my/74381/1/SIzman2016_OptimizationofChemicalPretreatment.pdf
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author Shah, A.
Izman, S.
Hassan, M. A.
Mustapha, R.
author_facet Shah, A.
Izman, S.
Hassan, M. A.
Mustapha, R.
author_sort Shah, A.
collection ePrints
description Diamond coating are commonly used in industries especially for application such as cutting tools, biomedical components, optical lenses, microelectronics, engineering, and thermal management systems. The diamond coating quality is strongly depending on substrate preparation prior to diamond coating. Thus, the several process parameters must be studied to obtain optimal parameters which lead high quality diamond coating. In this present work, an attempt was made to optimize pretreatment parameters namely temperature and time on cobalt removal of tungsten carbide. Full factorial experimental designs followed by Response Surface Methodology (RSM) were employed in this study to plan and analyze the experiment. The cobalt removal was the independent response variables. Empirical model was successfully developed to predict amount of cobalt removal on the substrate after single step etching process. Experimental results have shown that the temperature, time and time2 are found to be the most significant factors for cobalt removal. Whereas for interaction of time and temperature were insignificant factors to influence cobalt removal. According to this study, the minimum cobalt content can be obtained at working temperature from 48º to 50ºC for 3 minute.
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spelling utm.eprints-743812017-11-23T01:37:10Z http://eprints.utm.my/74381/ Optimization of chemical pretreatment for removing cobalt on tungsten carbide substrate using response surface methodology Shah, A. Izman, S. Hassan, M. A. Mustapha, R. TJ Mechanical engineering and machinery Diamond coating are commonly used in industries especially for application such as cutting tools, biomedical components, optical lenses, microelectronics, engineering, and thermal management systems. The diamond coating quality is strongly depending on substrate preparation prior to diamond coating. Thus, the several process parameters must be studied to obtain optimal parameters which lead high quality diamond coating. In this present work, an attempt was made to optimize pretreatment parameters namely temperature and time on cobalt removal of tungsten carbide. Full factorial experimental designs followed by Response Surface Methodology (RSM) were employed in this study to plan and analyze the experiment. The cobalt removal was the independent response variables. Empirical model was successfully developed to predict amount of cobalt removal on the substrate after single step etching process. Experimental results have shown that the temperature, time and time2 are found to be the most significant factors for cobalt removal. Whereas for interaction of time and temperature were insignificant factors to influence cobalt removal. According to this study, the minimum cobalt content can be obtained at working temperature from 48º to 50ºC for 3 minute. Penerbit UTM Press 2016 Article PeerReviewed application/pdf en http://eprints.utm.my/74381/1/SIzman2016_OptimizationofChemicalPretreatment.pdf Shah, A. and Izman, S. and Hassan, M. A. and Mustapha, R. (2016) Optimization of chemical pretreatment for removing cobalt on tungsten carbide substrate using response surface methodology. Jurnal Teknologi, 78 (5-10). pp. 16-32. ISSN 0127-9696 https://www.scopus.com/inward/record.uri?eid=2-s2.0-84971407780&doi=10.11113%2fjt.v78.8830&partnerID=40&md5=b1028262048f6774ec9febde59dd020c
spellingShingle TJ Mechanical engineering and machinery
Shah, A.
Izman, S.
Hassan, M. A.
Mustapha, R.
Optimization of chemical pretreatment for removing cobalt on tungsten carbide substrate using response surface methodology
title Optimization of chemical pretreatment for removing cobalt on tungsten carbide substrate using response surface methodology
title_full Optimization of chemical pretreatment for removing cobalt on tungsten carbide substrate using response surface methodology
title_fullStr Optimization of chemical pretreatment for removing cobalt on tungsten carbide substrate using response surface methodology
title_full_unstemmed Optimization of chemical pretreatment for removing cobalt on tungsten carbide substrate using response surface methodology
title_short Optimization of chemical pretreatment for removing cobalt on tungsten carbide substrate using response surface methodology
title_sort optimization of chemical pretreatment for removing cobalt on tungsten carbide substrate using response surface methodology
topic TJ Mechanical engineering and machinery
url http://eprints.utm.my/74381/1/SIzman2016_OptimizationofChemicalPretreatment.pdf
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AT izmans optimizationofchemicalpretreatmentforremovingcobaltontungstencarbidesubstrateusingresponsesurfacemethodology
AT hassanma optimizationofchemicalpretreatmentforremovingcobaltontungstencarbidesubstrateusingresponsesurfacemethodology
AT mustaphar optimizationofchemicalpretreatmentforremovingcobaltontungstencarbidesubstrateusingresponsesurfacemethodology