Development of hybrid coconut shell-peek adsorbent for methane adsorption: optimization using response surface methodology

Adsorbed natural gas (ANG) provides efficient and clean combustion, with minimal emissions compared to diesel and gasoline. This article was designed to develop techniques of ANG for transportation application by apply RSM and CCD to identify the optimum preparation conditions for preparation of sta...

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Main Authors: Sidik, H. U., Nasri, N. S., Rashid, N. M., Zaini, M. A. A., Abdulrahman, A., Zain, H. M.
Format: Article
Language:English
Published: Asian Research Publishing Network 2017
Subjects:
Online Access:http://eprints.utm.my/75376/1/NoorShawalNasri_DevelopmentofHybridCoconutShell-peek.pdf
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author Sidik, H. U.
Nasri, N. S.
Rashid, N. M.
Zaini, M. A. A.
Abdulrahman, A.
Zain, H. M.
author_facet Sidik, H. U.
Nasri, N. S.
Rashid, N. M.
Zaini, M. A. A.
Abdulrahman, A.
Zain, H. M.
author_sort Sidik, H. U.
collection ePrints
description Adsorbed natural gas (ANG) provides efficient and clean combustion, with minimal emissions compared to diesel and gasoline. This article was designed to develop techniques of ANG for transportation application by apply RSM and CCD to identify the optimum preparation conditions for preparation of stable adsorbent for methane adsorption. Coconut shell and poly ether ketone (PEEK) was selected for synthesis of activated carbon (AC). The effectiveness of the parameters was determined using response surface method (RSM) couple with central composite design (CCD). The analysis of variance (ANOVA) was applied to identify the significant parameters. The quadratic model was adopted, as it has the highest F-value of 21.62 and P-value of less than 0.05, which relate the parameters and response. Microwave power has the highest F-value of 62.36. The maximum methane uptake of 5.12mmol g-1 was achieved. Overall, the hybrid coconut-PEEK adsorbent was found to be suitable for CH4 adsorption.
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spelling utm.eprints-753762018-03-22T11:05:47Z http://eprints.utm.my/75376/ Development of hybrid coconut shell-peek adsorbent for methane adsorption: optimization using response surface methodology Sidik, H. U. Nasri, N. S. Rashid, N. M. Zaini, M. A. A. Abdulrahman, A. Zain, H. M. TP Chemical technology Adsorbed natural gas (ANG) provides efficient and clean combustion, with minimal emissions compared to diesel and gasoline. This article was designed to develop techniques of ANG for transportation application by apply RSM and CCD to identify the optimum preparation conditions for preparation of stable adsorbent for methane adsorption. Coconut shell and poly ether ketone (PEEK) was selected for synthesis of activated carbon (AC). The effectiveness of the parameters was determined using response surface method (RSM) couple with central composite design (CCD). The analysis of variance (ANOVA) was applied to identify the significant parameters. The quadratic model was adopted, as it has the highest F-value of 21.62 and P-value of less than 0.05, which relate the parameters and response. Microwave power has the highest F-value of 62.36. The maximum methane uptake of 5.12mmol g-1 was achieved. Overall, the hybrid coconut-PEEK adsorbent was found to be suitable for CH4 adsorption. Asian Research Publishing Network 2017 Article PeerReviewed application/pdf en http://eprints.utm.my/75376/1/NoorShawalNasri_DevelopmentofHybridCoconutShell-peek.pdf Sidik, H. U. and Nasri, N. S. and Rashid, N. M. and Zaini, M. A. A. and Abdulrahman, A. and Zain, H. M. (2017) Development of hybrid coconut shell-peek adsorbent for methane adsorption: optimization using response surface methodology. ARPN Journal of Engineering and Applied Sciences, 12 (20). pp. 5822-5829. ISSN 1819-6608 https://www.scopus.com/inward/record.uri?eid=2-s2.0-85032260209&partnerID=40&md5=e7e9f197e9b0f2d078bc88cb4a64ed2b
spellingShingle TP Chemical technology
Sidik, H. U.
Nasri, N. S.
Rashid, N. M.
Zaini, M. A. A.
Abdulrahman, A.
Zain, H. M.
Development of hybrid coconut shell-peek adsorbent for methane adsorption: optimization using response surface methodology
title Development of hybrid coconut shell-peek adsorbent for methane adsorption: optimization using response surface methodology
title_full Development of hybrid coconut shell-peek adsorbent for methane adsorption: optimization using response surface methodology
title_fullStr Development of hybrid coconut shell-peek adsorbent for methane adsorption: optimization using response surface methodology
title_full_unstemmed Development of hybrid coconut shell-peek adsorbent for methane adsorption: optimization using response surface methodology
title_short Development of hybrid coconut shell-peek adsorbent for methane adsorption: optimization using response surface methodology
title_sort development of hybrid coconut shell peek adsorbent for methane adsorption optimization using response surface methodology
topic TP Chemical technology
url http://eprints.utm.my/75376/1/NoorShawalNasri_DevelopmentofHybridCoconutShell-peek.pdf
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