Effects of dope extrusion rate on the morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes for 024 separation

The objective of this study was to investigate the influence of dope extrusion rates on morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes. Asymmetric poly- Sulfone hollow fiber membranes for gas separation were prepared from a solution consisting of 26.0 wt ....

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Main Authors: Ismail, Ahmad Fauzi, Mohd. Ibrahim, Suhaina, Nasri, Nor Shawal
Format: Article
Language:English
Published: Songkla University 2002
Subjects:
Online Access:http://eprints.utm.my/910/1/AhmadFauziIsmail2002_EffectsOfDopeExtrusionRate.pdf
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author Ismail, Ahmad Fauzi
Mohd. Ibrahim, Suhaina
Nasri, Nor Shawal
author_facet Ismail, Ahmad Fauzi
Mohd. Ibrahim, Suhaina
Nasri, Nor Shawal
author_sort Ismail, Ahmad Fauzi
collection ePrints
description The objective of this study was to investigate the influence of dope extrusion rates on morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes. Asymmetric poly- Sulfone hollow fiber membranes for gas separation were prepared from a solution consisting of 26.0 wt . % ofpolysulfone, 30.4 wt. % of N, N-dhnethylacetamide, 30.4 wt. % of tetrahydrofuran and 13.2 wt. % ethanol. The dry/wet phase separation process was applied to a drylwet spinning process. Fibers were spun at various dope extrusion rates (DER) ranging from 1.5 - 3.0 cm3/min and hence at different levels of shear. The results Suggest that as the dope extrusion rate is increased, the selectivity will increase until a critical level of shear is reached, beyond which the membrane performance deteriorates. Pressure-normalized-fluxes and selectivities were evaluated by using pure oxygen and nitrogen as test gases.
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spelling utm.eprints-9102010-10-25T08:14:28Z http://eprints.utm.my/910/ Effects of dope extrusion rate on the morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes for 024 separation Ismail, Ahmad Fauzi Mohd. Ibrahim, Suhaina Nasri, Nor Shawal TP Chemical technology The objective of this study was to investigate the influence of dope extrusion rates on morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes. Asymmetric poly- Sulfone hollow fiber membranes for gas separation were prepared from a solution consisting of 26.0 wt . % ofpolysulfone, 30.4 wt. % of N, N-dhnethylacetamide, 30.4 wt. % of tetrahydrofuran and 13.2 wt. % ethanol. The dry/wet phase separation process was applied to a drylwet spinning process. Fibers were spun at various dope extrusion rates (DER) ranging from 1.5 - 3.0 cm3/min and hence at different levels of shear. The results Suggest that as the dope extrusion rate is increased, the selectivity will increase until a critical level of shear is reached, beyond which the membrane performance deteriorates. Pressure-normalized-fluxes and selectivities were evaluated by using pure oxygen and nitrogen as test gases. Songkla University 2002 Article PeerReviewed application/pdf en http://eprints.utm.my/910/1/AhmadFauziIsmail2002_EffectsOfDopeExtrusionRate.pdf Ismail, Ahmad Fauzi and Mohd. Ibrahim, Suhaina and Nasri, Nor Shawal (2002) Effects of dope extrusion rate on the morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes for 024 separation. Songklanakarin Journal of Science and Technology, 24 (Suppl). pp. 833-842. ISSN 0125-3395 http://www.rdoapp.psu.ac.th/html/sjst/journal/24-Suppl-1/09gas.pdf
spellingShingle TP Chemical technology
Ismail, Ahmad Fauzi
Mohd. Ibrahim, Suhaina
Nasri, Nor Shawal
Effects of dope extrusion rate on the morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes for 024 separation
title Effects of dope extrusion rate on the morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes for 024 separation
title_full Effects of dope extrusion rate on the morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes for 024 separation
title_fullStr Effects of dope extrusion rate on the morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes for 024 separation
title_full_unstemmed Effects of dope extrusion rate on the morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes for 024 separation
title_short Effects of dope extrusion rate on the morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes for 024 separation
title_sort effects of dope extrusion rate on the morphology and gas separation performance of asymmetric polysulfone hollow fiber membranes for 024 separation
topic TP Chemical technology
url http://eprints.utm.my/910/1/AhmadFauziIsmail2002_EffectsOfDopeExtrusionRate.pdf
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AT mohdibrahimsuhaina effectsofdopeextrusionrateonthemorphologyandgasseparationperformanceofasymmetricpolysulfonehollowfibermembranesfor024separation
AT nasrinorshawal effectsofdopeextrusionrateonthemorphologyandgasseparationperformanceofasymmetricpolysulfonehollowfibermembranesfor024separation