Optimization of pectin extraction from sweet potato peels using citric acid and its emulsifying properties

Background: Pectin is a natural polysaccharide that has been used widely as a stabilizer in food emulsion system. Objective: This study aimed to optimize the yield of pectin extracted from sweet potato residue and investigate its emulsifying properties. Methods: Response surface methodology (RSM) ha...

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Main Authors: Hamidon, N. H., Zaidel, D. N. A., Jusoh, Y. M. M.
Format: Article
Published: Bentham Science Publishers 2020
Subjects:
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author Hamidon, N. H.
Zaidel, D. N. A.
Jusoh, Y. M. M.
author_facet Hamidon, N. H.
Zaidel, D. N. A.
Jusoh, Y. M. M.
author_sort Hamidon, N. H.
collection ePrints
description Background: Pectin is a natural polysaccharide that has been used widely as a stabilizer in food emulsion system. Objective: This study aimed to optimize the yield of pectin extracted from sweet potato residue and investigate its emulsifying properties. Methods: Response surface methodology (RSM) has been utilized to investigate the pectin extracted from sweet potato peels using citric acid as the extracting solvent. Investigation of the effect of different extraction conditions namely temperature (°C), time (min) and solution pH on pectin yield (%) were conducted. A Box-Benhken design with three levels of variation was used to optimize the extraction conditions. Results: The optimal conditions determined were temperature 76°C, time 64 min and pH 1.2 with 65.2% yield of pectin. The degree of esterification (DE) of the sweet potato pectin was determined using Fourier Transform Infrared (FTIR) Spectroscopy. The pectin is high-methoxyl pectin with DE of 58.5%. Emulsifying properties of sweet potato pectin were investigated by measuring the zeta-potential, particle size and creaming index with addition of 0.4 and 1.0 wt % pectin to the emulsion. Conclusion: Extraction using citric acid could improve the pectin yield. Improved emulsion stability was observed with the addition of the sweet potato pectin.
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spelling utm.eprints-928572021-10-28T10:13:30Z http://eprints.utm.my/92857/ Optimization of pectin extraction from sweet potato peels using citric acid and its emulsifying properties Hamidon, N. H. Zaidel, D. N. A. Jusoh, Y. M. M. TP Chemical technology Background: Pectin is a natural polysaccharide that has been used widely as a stabilizer in food emulsion system. Objective: This study aimed to optimize the yield of pectin extracted from sweet potato residue and investigate its emulsifying properties. Methods: Response surface methodology (RSM) has been utilized to investigate the pectin extracted from sweet potato peels using citric acid as the extracting solvent. Investigation of the effect of different extraction conditions namely temperature (°C), time (min) and solution pH on pectin yield (%) were conducted. A Box-Benhken design with three levels of variation was used to optimize the extraction conditions. Results: The optimal conditions determined were temperature 76°C, time 64 min and pH 1.2 with 65.2% yield of pectin. The degree of esterification (DE) of the sweet potato pectin was determined using Fourier Transform Infrared (FTIR) Spectroscopy. The pectin is high-methoxyl pectin with DE of 58.5%. Emulsifying properties of sweet potato pectin were investigated by measuring the zeta-potential, particle size and creaming index with addition of 0.4 and 1.0 wt % pectin to the emulsion. Conclusion: Extraction using citric acid could improve the pectin yield. Improved emulsion stability was observed with the addition of the sweet potato pectin. Bentham Science Publishers 2020 Article PeerReviewed Hamidon, N. H. and Zaidel, D. N. A. and Jusoh, Y. M. M. (2020) Optimization of pectin extraction from sweet potato peels using citric acid and its emulsifying properties. Recent Patents on Food, Nutrition and Agriculture, 11 (3). ISSN 2212-7984 http://dx.doi.org/10.2174/2212798411666200207102051 DOI: 10.2174/2212798411666200207102051
spellingShingle TP Chemical technology
Hamidon, N. H.
Zaidel, D. N. A.
Jusoh, Y. M. M.
Optimization of pectin extraction from sweet potato peels using citric acid and its emulsifying properties
title Optimization of pectin extraction from sweet potato peels using citric acid and its emulsifying properties
title_full Optimization of pectin extraction from sweet potato peels using citric acid and its emulsifying properties
title_fullStr Optimization of pectin extraction from sweet potato peels using citric acid and its emulsifying properties
title_full_unstemmed Optimization of pectin extraction from sweet potato peels using citric acid and its emulsifying properties
title_short Optimization of pectin extraction from sweet potato peels using citric acid and its emulsifying properties
title_sort optimization of pectin extraction from sweet potato peels using citric acid and its emulsifying properties
topic TP Chemical technology
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AT zaideldna optimizationofpectinextractionfromsweetpotatopeelsusingcitricacidanditsemulsifyingproperties
AT jusohymm optimizationofpectinextractionfromsweetpotatopeelsusingcitricacidanditsemulsifyingproperties