Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes

In the past few years, composite membrane has been introduced to cater the limitation of polymeric and inorganic membranes. However, the fabrication of ideal composite membrane with appropriate loading of filler remains challenging. Thus, the material selection as well as optimum loading with the co...

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Main Authors: Kamarudin, Mohd. Syazwan, Jusoh, Norwahyu, Tengku Hassan, Tengku Nur Adibah, Md. Ali, Umi Fazara, Abdullah, Syamsul Bahari, Amir Hamzah, Amir Syafiq Syamin Syah
Format: Conference or Workshop Item
Published: 2021
Subjects:
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author Kamarudin, Mohd. Syazwan
Jusoh, Norwahyu
Tengku Hassan, Tengku Nur Adibah
Md. Ali, Umi Fazara
Abdullah, Syamsul Bahari
Amir Hamzah, Amir Syafiq Syamin Syah
author_facet Kamarudin, Mohd. Syazwan
Jusoh, Norwahyu
Tengku Hassan, Tengku Nur Adibah
Md. Ali, Umi Fazara
Abdullah, Syamsul Bahari
Amir Hamzah, Amir Syafiq Syamin Syah
author_sort Kamarudin, Mohd. Syazwan
collection ePrints
description In the past few years, composite membrane has been introduced to cater the limitation of polymeric and inorganic membranes. However, the fabrication of ideal composite membrane with appropriate loading of filler remains challenging. Thus, the material selection as well as optimum loading with the conditions observed for the formulation of the composite membrane studied. In this present work, a series of poly (ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membrane with different loading of SAPO-34 particles (0-4 wt%) were fabricated. The physicochemical properties of the resultant membranes were investigated by utilizing X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive X-ray (EDX). Based on analysis, a good distribution of filler was obtained for the membranes loaded with 1 wt% and 2 wt% of SAPO-34 particles. Further increase of inorganic filler loading lead to the sedimentation and agglomeration of particle in the membrane, which may deteriorate the membrane performance in gas separation. Therefore, the optimum loading of inorganic particles in polymer phase play a major role in obtaining membrane with minimum defects ahead of gas separation performance tests such as for CO2/ethylene separation application.
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spelling utm.eprints-960082022-07-01T08:16:08Z http://eprints.utm.my/96008/ Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes Kamarudin, Mohd. Syazwan Jusoh, Norwahyu Tengku Hassan, Tengku Nur Adibah Md. Ali, Umi Fazara Abdullah, Syamsul Bahari Amir Hamzah, Amir Syafiq Syamin Syah Q Science (General) In the past few years, composite membrane has been introduced to cater the limitation of polymeric and inorganic membranes. However, the fabrication of ideal composite membrane with appropriate loading of filler remains challenging. Thus, the material selection as well as optimum loading with the conditions observed for the formulation of the composite membrane studied. In this present work, a series of poly (ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membrane with different loading of SAPO-34 particles (0-4 wt%) were fabricated. The physicochemical properties of the resultant membranes were investigated by utilizing X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive X-ray (EDX). Based on analysis, a good distribution of filler was obtained for the membranes loaded with 1 wt% and 2 wt% of SAPO-34 particles. Further increase of inorganic filler loading lead to the sedimentation and agglomeration of particle in the membrane, which may deteriorate the membrane performance in gas separation. Therefore, the optimum loading of inorganic particles in polymer phase play a major role in obtaining membrane with minimum defects ahead of gas separation performance tests such as for CO2/ethylene separation application. 2021 Conference or Workshop Item PeerReviewed Kamarudin, Mohd. Syazwan and Jusoh, Norwahyu and Tengku Hassan, Tengku Nur Adibah and Md. Ali, Umi Fazara and Abdullah, Syamsul Bahari and Amir Hamzah, Amir Syafiq Syamin Syah (2021) Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes. In: 3rd International Conference on Separation Technology (ICoST), 15 August 2020 - 16 August 2020, Virtual, Online. http://dx.doi.org/10.1016/j.matpr.2021.02.793
spellingShingle Q Science (General)
Kamarudin, Mohd. Syazwan
Jusoh, Norwahyu
Tengku Hassan, Tengku Nur Adibah
Md. Ali, Umi Fazara
Abdullah, Syamsul Bahari
Amir Hamzah, Amir Syafiq Syamin Syah
Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes
title Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes
title_full Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes
title_fullStr Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes
title_full_unstemmed Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes
title_short Fabrication and characterization of poly(ether-block-amide) (Pebax-1657) and silicoaluminophosphate (SAPO-34) composite membranes
title_sort fabrication and characterization of poly ether block amide pebax 1657 and silicoaluminophosphate sapo 34 composite membranes
topic Q Science (General)
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