Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design

Experimental design (ED) is a powerful technique for optimizing the performance of a process. Compared to a model-based optimization technique, ED does not require the development of mathematical formulation but nevertheless needs a good model or experimental setup and statistical analysis. This pap...

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Main Authors: Mohamad Rizza, Othman, Umarul Imran, Amran, Gade Padu, Rangaiah
Format: Article
Language:English
English
Published: AIDIC Servizi 2015
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/12837/1/0253_CET45_155.pdf
http://umpir.ump.edu.my/id/eprint/12837/2/Process%20Optimization%20of%20DWC%20for%20Fatty%20Acid%20Fractionation%20using%20Taguchi%20Methods%20of%20Experimental%20Design.pdf
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author Mohamad Rizza, Othman
Umarul Imran, Amran
Gade Padu, Rangaiah
author_facet Mohamad Rizza, Othman
Umarul Imran, Amran
Gade Padu, Rangaiah
author_sort Mohamad Rizza, Othman
collection UMP
description Experimental design (ED) is a powerful technique for optimizing the performance of a process. Compared to a model-based optimization technique, ED does not require the development of mathematical formulation but nevertheless needs a good model or experimental setup and statistical analysis. This paper presents an ED based optimization approach of a dividing wall column (DWC) model for industrial oleochemical fatty acid fractionation. Taguchi method of ED will be used for the optimization of the control variables for efficient fractionation of fatty acid cuts, namely light-cut (LC), middle-cut (MC) and heavy-cut (HC). The DWC model was developed in Aspen Plus software using a rigorous four-column configuration. It is used to identify sensitive parameters, simulate experimental layout trials and results validation. The process is designed to achieve product purity of >99 mol.% LC and MC, and >90 mol.% for HC. A step-by-step approach to process optimization using Taguchi method is presented along with the statistical analysis results and their interpretation. The ED output will help in understanding the interaction between variables and their effects. With its simple, fast and non-tedious approach, ED using Taguchi method could prove its significance in improving the performance of fatty acid fractionation using DWC for possible industrial application.
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spelling UMPir128372018-03-09T07:16:03Z http://umpir.ump.edu.my/id/eprint/12837/ Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design Mohamad Rizza, Othman Umarul Imran, Amran Gade Padu, Rangaiah TP Chemical technology Experimental design (ED) is a powerful technique for optimizing the performance of a process. Compared to a model-based optimization technique, ED does not require the development of mathematical formulation but nevertheless needs a good model or experimental setup and statistical analysis. This paper presents an ED based optimization approach of a dividing wall column (DWC) model for industrial oleochemical fatty acid fractionation. Taguchi method of ED will be used for the optimization of the control variables for efficient fractionation of fatty acid cuts, namely light-cut (LC), middle-cut (MC) and heavy-cut (HC). The DWC model was developed in Aspen Plus software using a rigorous four-column configuration. It is used to identify sensitive parameters, simulate experimental layout trials and results validation. The process is designed to achieve product purity of >99 mol.% LC and MC, and >90 mol.% for HC. A step-by-step approach to process optimization using Taguchi method is presented along with the statistical analysis results and their interpretation. The ED output will help in understanding the interaction between variables and their effects. With its simple, fast and non-tedious approach, ED using Taguchi method could prove its significance in improving the performance of fatty acid fractionation using DWC for possible industrial application. AIDIC Servizi 2015 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/12837/1/0253_CET45_155.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/12837/2/Process%20Optimization%20of%20DWC%20for%20Fatty%20Acid%20Fractionation%20using%20Taguchi%20Methods%20of%20Experimental%20Design.pdf Mohamad Rizza, Othman and Umarul Imran, Amran and Gade Padu, Rangaiah (2015) Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design. Chemical Engineering Transactions, 45. pp. 925-930. ISSN 2283-9216. (Published) http://dx.doi.org/10.3303/CET1545155 DOI: 10.3303/CET1545155
spellingShingle TP Chemical technology
Mohamad Rizza, Othman
Umarul Imran, Amran
Gade Padu, Rangaiah
Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design
title Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design
title_full Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design
title_fullStr Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design
title_full_unstemmed Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design
title_short Process Optimization of DWC for Fatty Acid Fractionation using Taguchi Methods of Experimental Design
title_sort process optimization of dwc for fatty acid fractionation using taguchi methods of experimental design
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/12837/1/0253_CET45_155.pdf
http://umpir.ump.edu.my/id/eprint/12837/2/Process%20Optimization%20of%20DWC%20for%20Fatty%20Acid%20Fractionation%20using%20Taguchi%20Methods%20of%20Experimental%20Design.pdf
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