Microstructural Evolution in a 0.09% Niobium Low Carbon Steel during Controlled Hot Deformation

A series of plane strain compression tests were carried out in order to simulate the thermomechanical controlled processing of a 0.09wt% Nb low carbon steel, in a scheme of multipass finish rolling at 950 °C with interpass times of 10 s. It was observed that after the first two finishing passes a re...

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Main Authors: E. Pineda Martínez, E. J. Palmiere
Format: Article
Language:English
Published: MDPI AG 2024-02-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/14/3/283
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author E. Pineda Martínez
E. J. Palmiere
author_facet E. Pineda Martínez
E. J. Palmiere
author_sort E. Pineda Martínez
collection DOAJ
description A series of plane strain compression tests were carried out in order to simulate the thermomechanical controlled processing of a 0.09wt% Nb low carbon steel, in a scheme of multipass finish rolling at 950 °C with interpass times of 10 s. It was observed that after the first two finishing passes a remarkable grain refinement can be achieved, since the recrystallisation was fully suppressed and abundant ultrafine ferrite was transformed dynamically during the deformation. The addition of a third finishing pass however, led to partial recrystallisation. A deep characterisation of the dynamic ferrite was carried out by diverse methods conducting to relevant findings that contribute to a better elucidation of the dynamic transformation. The results obtained indicated that the dynamic formation of a colony of Widmanstätten ferrite plates during deformation, initiates with the formation of a pair of self-accommodating plates followed by face-to-face sympathetic nucleation of new plates at one of the faces of the pairs of plates already formed. Furthermore, the crystal orientation within the dynamic ferrite phase was analysed with EBSD, it was observed that during the coalescence of plates, prior to the full polygonisation of grains, the ferrite adopts a transitory morphology which possesses particular crystallographic characteristics.
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spelling doaj.art-16241a691e204dadb903afb255fc729a2024-03-27T13:54:19ZengMDPI AGMetals2075-47012024-02-0114328310.3390/met14030283Microstructural Evolution in a 0.09% Niobium Low Carbon Steel during Controlled Hot DeformationE. Pineda Martínez0E. J. Palmiere1Department of Materials Science and Engineering, The University of Sheffield, Sir Robert Hadfield Building, Mappin Street, Sheffield S1 3JD, UKDepartment of Materials Science and Engineering, The University of Sheffield, Sir Robert Hadfield Building, Mappin Street, Sheffield S1 3JD, UKA series of plane strain compression tests were carried out in order to simulate the thermomechanical controlled processing of a 0.09wt% Nb low carbon steel, in a scheme of multipass finish rolling at 950 °C with interpass times of 10 s. It was observed that after the first two finishing passes a remarkable grain refinement can be achieved, since the recrystallisation was fully suppressed and abundant ultrafine ferrite was transformed dynamically during the deformation. The addition of a third finishing pass however, led to partial recrystallisation. A deep characterisation of the dynamic ferrite was carried out by diverse methods conducting to relevant findings that contribute to a better elucidation of the dynamic transformation. The results obtained indicated that the dynamic formation of a colony of Widmanstätten ferrite plates during deformation, initiates with the formation of a pair of self-accommodating plates followed by face-to-face sympathetic nucleation of new plates at one of the faces of the pairs of plates already formed. Furthermore, the crystal orientation within the dynamic ferrite phase was analysed with EBSD, it was observed that during the coalescence of plates, prior to the full polygonisation of grains, the ferrite adopts a transitory morphology which possesses particular crystallographic characteristics.https://www.mdpi.com/2075-4701/14/3/283ultrafine steeldynamic ferrite transformationmicrostructural evolutionthermomechanical controlled processing (TMCP)
spellingShingle E. Pineda Martínez
E. J. Palmiere
Microstructural Evolution in a 0.09% Niobium Low Carbon Steel during Controlled Hot Deformation
Metals
ultrafine steel
dynamic ferrite transformation
microstructural evolution
thermomechanical controlled processing (TMCP)
title Microstructural Evolution in a 0.09% Niobium Low Carbon Steel during Controlled Hot Deformation
title_full Microstructural Evolution in a 0.09% Niobium Low Carbon Steel during Controlled Hot Deformation
title_fullStr Microstructural Evolution in a 0.09% Niobium Low Carbon Steel during Controlled Hot Deformation
title_full_unstemmed Microstructural Evolution in a 0.09% Niobium Low Carbon Steel during Controlled Hot Deformation
title_short Microstructural Evolution in a 0.09% Niobium Low Carbon Steel during Controlled Hot Deformation
title_sort microstructural evolution in a 0 09 niobium low carbon steel during controlled hot deformation
topic ultrafine steel
dynamic ferrite transformation
microstructural evolution
thermomechanical controlled processing (TMCP)
url https://www.mdpi.com/2075-4701/14/3/283
work_keys_str_mv AT epinedamartinez microstructuralevolutionina009niobiumlowcarbonsteelduringcontrolledhotdeformation
AT ejpalmiere microstructuralevolutionina009niobiumlowcarbonsteelduringcontrolledhotdeformation