Characterization of antimicrobial multilayer film based on ethylcellulose-pectin incorporated with nanoemulsions of trans-cinnamaldehyde essential oil

In this study, polymer solution casting was utilized to fabricate a multilayer film with ethylcellulose (EC) as the outer layers and trans-cinnamaldehyde-loaded pectin as the inner layer. A significant increase in whiteness and UV–visible light blocking capability and a remarkable decrease in total...

Full description

Bibliographic Details
Main Authors: Fatemeh Baghi, Adem Gharsallaoui, Emilie Dumas, Géraldine Agusti, Sami Ghnimi
Format: Article
Language:English
Published: Elsevier 2024-06-01
Series:Food Chemistry: X
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2590157524001482
_version_ 1797268957819830272
author Fatemeh Baghi
Adem Gharsallaoui
Emilie Dumas
Géraldine Agusti
Sami Ghnimi
author_facet Fatemeh Baghi
Adem Gharsallaoui
Emilie Dumas
Géraldine Agusti
Sami Ghnimi
author_sort Fatemeh Baghi
collection DOAJ
description In this study, polymer solution casting was utilized to fabricate a multilayer film with ethylcellulose (EC) as the outer layers and trans-cinnamaldehyde-loaded pectin as the inner layer. A significant increase in whiteness and UV–visible light blocking capability and a remarkable decrease in total color difference and yellowness of the films were seen via increasing the thickness of EC outer layers. Scanning electronic microscopy observation showed that the inner and outer layers had a smooth and uniform surfaces with clear boundary. The thicker film has better stretchability and strength, but is less flexible than thinner film. Glass transition temperature did not change remarkably with increasing thickness of EC outer layers, but thermal stability was slightly improved. FTIR-ATR spectra revealed the formation of hydrogen bonds between the two adjacent layers. The multilayer films exhibited excellent antimicrobial efficacy against Gram-positive and Gram-negative foodborne pathogens. The results suggested that this multilayer film has potential applications in active food packaging.
first_indexed 2024-04-25T01:40:44Z
format Article
id doaj.art-1a3f30c61fce456ea3381fcbbc96cad8
institution Directory Open Access Journal
issn 2590-1575
language English
last_indexed 2024-04-25T01:40:44Z
publishDate 2024-06-01
publisher Elsevier
record_format Article
series Food Chemistry: X
spelling doaj.art-1a3f30c61fce456ea3381fcbbc96cad82024-03-08T05:19:17ZengElsevierFood Chemistry: X2590-15752024-06-0122101261Characterization of antimicrobial multilayer film based on ethylcellulose-pectin incorporated with nanoemulsions of trans-cinnamaldehyde essential oilFatemeh Baghi0Adem Gharsallaoui1Emilie Dumas2Géraldine Agusti3Sami Ghnimi4Univ Lyon, Université Claude Bernard Lyon 1, LAGEPP UMR 5007, F-69622, Villeurbanne, France; ISARA, 23 Rue Jean Baldassini, 69007 Lyon, FranceUniv Lyon, Université Claude Bernard Lyon 1, LAGEPP UMR 5007, F-69622, Villeurbanne, FranceUniv Lyon, Université Claude Bernard Lyon 1, LAGEPP UMR 5007, F-69622, Villeurbanne, FranceUniv Lyon, Université Claude Bernard Lyon 1, LAGEPP UMR 5007, F-69622, Villeurbanne, FranceUniv Lyon, Université Claude Bernard Lyon 1, LAGEPP UMR 5007, F-69622, Villeurbanne, France; ISARA, 23 Rue Jean Baldassini, 69007 Lyon, France; Corresponding author at: Univ Lyon, Université Claude Bernard Lyon 1, LAGEPP UMR 5007, F-69622, Villeurbanne, France.In this study, polymer solution casting was utilized to fabricate a multilayer film with ethylcellulose (EC) as the outer layers and trans-cinnamaldehyde-loaded pectin as the inner layer. A significant increase in whiteness and UV–visible light blocking capability and a remarkable decrease in total color difference and yellowness of the films were seen via increasing the thickness of EC outer layers. Scanning electronic microscopy observation showed that the inner and outer layers had a smooth and uniform surfaces with clear boundary. The thicker film has better stretchability and strength, but is less flexible than thinner film. Glass transition temperature did not change remarkably with increasing thickness of EC outer layers, but thermal stability was slightly improved. FTIR-ATR spectra revealed the formation of hydrogen bonds between the two adjacent layers. The multilayer films exhibited excellent antimicrobial efficacy against Gram-positive and Gram-negative foodborne pathogens. The results suggested that this multilayer film has potential applications in active food packaging.http://www.sciencedirect.com/science/article/pii/S2590157524001482EthylcellulosePectinMultilayer filmNanoemulsionAntimicrobial activityActive packaging
spellingShingle Fatemeh Baghi
Adem Gharsallaoui
Emilie Dumas
Géraldine Agusti
Sami Ghnimi
Characterization of antimicrobial multilayer film based on ethylcellulose-pectin incorporated with nanoemulsions of trans-cinnamaldehyde essential oil
Food Chemistry: X
Ethylcellulose
Pectin
Multilayer film
Nanoemulsion
Antimicrobial activity
Active packaging
title Characterization of antimicrobial multilayer film based on ethylcellulose-pectin incorporated with nanoemulsions of trans-cinnamaldehyde essential oil
title_full Characterization of antimicrobial multilayer film based on ethylcellulose-pectin incorporated with nanoemulsions of trans-cinnamaldehyde essential oil
title_fullStr Characterization of antimicrobial multilayer film based on ethylcellulose-pectin incorporated with nanoemulsions of trans-cinnamaldehyde essential oil
title_full_unstemmed Characterization of antimicrobial multilayer film based on ethylcellulose-pectin incorporated with nanoemulsions of trans-cinnamaldehyde essential oil
title_short Characterization of antimicrobial multilayer film based on ethylcellulose-pectin incorporated with nanoemulsions of trans-cinnamaldehyde essential oil
title_sort characterization of antimicrobial multilayer film based on ethylcellulose pectin incorporated with nanoemulsions of trans cinnamaldehyde essential oil
topic Ethylcellulose
Pectin
Multilayer film
Nanoemulsion
Antimicrobial activity
Active packaging
url http://www.sciencedirect.com/science/article/pii/S2590157524001482
work_keys_str_mv AT fatemehbaghi characterizationofantimicrobialmultilayerfilmbasedonethylcellulosepectinincorporatedwithnanoemulsionsoftranscinnamaldehydeessentialoil
AT ademgharsallaoui characterizationofantimicrobialmultilayerfilmbasedonethylcellulosepectinincorporatedwithnanoemulsionsoftranscinnamaldehydeessentialoil
AT emiliedumas characterizationofantimicrobialmultilayerfilmbasedonethylcellulosepectinincorporatedwithnanoemulsionsoftranscinnamaldehydeessentialoil
AT geraldineagusti characterizationofantimicrobialmultilayerfilmbasedonethylcellulosepectinincorporatedwithnanoemulsionsoftranscinnamaldehydeessentialoil
AT samighnimi characterizationofantimicrobialmultilayerfilmbasedonethylcellulosepectinincorporatedwithnanoemulsionsoftranscinnamaldehydeessentialoil