Development of a versatile electrochemical cell for in situ grazing-incidence X-ray diffraction during non-aqueous electrochemical nitrogen reduction

Development of a versatile electrochemical cell for in situ grazing-incidence X-ray diffraction during non-aqueous electrochemical nitrogen reduction

In situ techniques are essential to understanding the behavior of electrocatalysts under operating conditions. When employed, in situ synchrotron grazing-incidence X-ray diffraction (GI-XRD) can provide time-resolved structural information of materials formed at the electrode surface. In situ cells,...

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Bibliographic Details
Main Authors: Sarah J. Blair, Adam C. Nielander, Kevin H. Stone, Melissa E. Kreider, Valerie A. Niemann, Peter Benedek, Eric J. McShane, Alessandro Gallo, Thomas F. Jaramillo
Format: Article
Language:English
Published: International Union of Crystallography 2023-09-01
Series:Journal of Synchrotron Radiation
Subjects:
non-aqueous li-mediated electrochemical nitrogen reduction
synchrotron x-ray diffraction
electrocatalysis
electrochemical cell design
grazing incidence
in situ
solid electrolyte interphase
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600577523006331

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http://scripts.iucr.org/cgi-bin/paper?S1600577523006331

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