Syntheses and crystal structures of two dinaphtho[2,1-d:1′,2′-f][1,3]dithiepine atropisomers

Syntheses and crystal structures of two dinaphtho[2,1-d:1′,2′-f][1,3]dithiepine atropisomers

The closely related title compounds, 1-(dinaphtho[2,1-d:1′,2′-f][1,3]dithiepin-4-yl)-2,2-dimethylpropan-1-ol, C26H24OS2, 1 and 2-(dinaphtho[2,1-d:1′,2′-f][1,3]dithiepin-4-yl)-3,3-dimethylbutan-2-ol, C27H26OS2, 2, both comprise an atropisomeric binaphthyl dithioacetal unit substituted at the methylen...

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Bibliographic Details
Main Authors: Neil Beare, Gavin F. Painter, C. John McAdam
Format: Article
Language:English
Published: International Union of Crystallography 2023-02-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
atropisomer
binaphthalene dithiol
asymmetric synthesis
hydrogen bonds
c—h...π contacts
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989023000476

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http://scripts.iucr.org/cgi-bin/paper?S2056989023000476

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