Syntheses and crystal structures of 4-(4-nitrophenyl)piperazin-1-ium benzoate monohydrate and 4-(4-nitrophenyl)piperazin-1-ium 2-carboxy-4,6-dinitrophenolate

Syntheses and crystal structures of 4-(4-nitrophenyl)piperazin-1-ium benzoate monohydrate and 4-(4-nitrophenyl)piperazin-1-ium 2-carboxy-4,6-dinitrophenolate

Crystal structures are reported for two molecular salts containing the 4-(4-nitrophenyl)piperazin-1-ium cation. Co-crystallization from methanol/ethyl acetate solution of N-(4-nitrophenyl)piperazine with benzoic acid gives the benzoate salt, which crystallizes as a monohydrate, C10H14N3O2·C7H5O2·H2O...

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Bibliographic Details
Main Authors: Holehundi J. Shankara Prasad, Devaraju, Vinaya, Hemmige S. Yathirajan, Sean R. Parkin, Christopher Glidewell
Format: Article
Language:English
Published: International Union of Crystallography 2022-08-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
piperazine
synthesis
crystal structure
molecular structure
hydrogen bonding
supramolecular assembly
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989022007472

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http://scripts.iucr.org/cgi-bin/paper?S2056989022007472

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