Redetermination of the structure of 2-amino-8-thia-1,5-diazaspiro[4.5]dec-1-en-5-ium chloride monohydrate

Redetermination of the structure of 2-amino-8-thia-1,5-diazaspiro[4.5]dec-1-en-5-ium chloride monohydrate

The reaction of β-(thiomorpholin-1-yl)propioamidoxime with tosyl chloride in CHCl3 in the presence of DIPEA when heated at 343 K for 8 h afforded the title hydrated salt, C7H14N3S+·Cl−·H2O, in 84% yield. This course of the tosylation reaction differs from the result of tosylation obtained for this s...

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Bibliographic Details
Main Authors: Lyudmila A. Kayukova, Elmira M. Yergaliyeva, Anna V. Vologzhanina
Format: Article
Language:English
Published: International Union of Crystallography 2022-02-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
hydrogen bonding
redetermination
spiro[4.5]dec-1-en-5-ium
tosylation
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989022000111

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http://scripts.iucr.org/cgi-bin/paper?S2056989022000111

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