Optimization of Extraction Process and Component Analysis of Oleoresin from Smoked Amomum tsaoko by Response Surface Methodology
In order to obtain the best extraction process of smoked Amomum tsaoko(SDAT) oleoresin, the extraction solvent, extraction temperature, solid-liquid ratio, extraction time and particle size were regarded as the influence factors. On the basis of single factor experiment, the eexperimental design of...
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The editorial department of Science and Technology of Food Industry
2022-01-01
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| Series: | Shipin gongye ke-ji |
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| Online Access: | http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2021040002 |
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| author | Yi LIN Mei HUANG Guiping WU Fei XU Juncai HE Shengjun YOU Penghui GAO Linna LIU Meifang HOU Fenglin GU |
| author_facet | Yi LIN Mei HUANG Guiping WU Fei XU Juncai HE Shengjun YOU Penghui GAO Linna LIU Meifang HOU Fenglin GU |
| author_sort | Yi LIN |
| collection | DOAJ |
| description | In order to obtain the best extraction process of smoked Amomum tsaoko(SDAT) oleoresin, the extraction solvent, extraction temperature, solid-liquid ratio, extraction time and particle size were regarded as the influence factors. On the basis of single factor experiment, the eexperimental design of three factors and three levels was used by Box-Benhnken central composite method, according to the extraction rate of SDAT oleoresin as the response value, and the extraction conditions were further optimized by response surface methodology(RSM). The results showed that the optimum process conditions of SDAT oleoresin was as follows: Anhydrous methanol as solvent, extraction temperature was 75 ℃, solid-liquidratio was 1:20(g/mL), extraction time was 7 h and particle size was 80 mesh. The regression equation predicted that the theoretical extraction rate of SDAT could reach 9.57%, the average extraction rate of the three validation experiments was 9.48%, and the predicted value was close to the actual result. And 58 compounds were identified by GC-TOF-MS, including alcohols(31.59%), aldehydes(21.13%), alkenes(1.23%), ketones(1.56%), esters(2.38%) and phenols(0.79%), 1,8-eucalyptol(9.28%), α-terpineol(3.55%), gera-niol(8.4%), trans citral(5.78%), 2-methyl-3-ph-enylpropanal(6.33%), etc. Through the determination of the best process of SDAT oleoresin, the detected components are mainly concentrated in alcohols and aldehydes, which provides a theoretical basis for the nutritional components and biological activity of grass fruit oleoresin in the later stage. |
| first_indexed | 2024-04-12T10:43:27Z |
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| id | doaj.art-4c4e5a689c6c447eb9e60a32f164188d |
| institution | Directory Open Access Journal |
| issn | 1002-0306 |
| language | zho |
| last_indexed | 2024-04-12T10:43:27Z |
| publishDate | 2022-01-01 |
| publisher | The editorial department of Science and Technology of Food Industry |
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| series | Shipin gongye ke-ji |
| spelling | doaj.art-4c4e5a689c6c447eb9e60a32f164188d2022-12-22T03:36:31ZzhoThe editorial department of Science and Technology of Food IndustryShipin gongye ke-ji1002-03062022-01-0143116317110.13386/j.issn1002-0306.20210400022021040002-1Optimization of Extraction Process and Component Analysis of Oleoresin from Smoked Amomum tsaoko by Response Surface MethodologyYi LIN0Mei HUANG1Guiping WU2Fei XU3Juncai HE4Shengjun YOU5Penghui GAO6Linna LIU7Meifang HOU8Fenglin GU9School of Ecological Technology and Engineering, Shanghai Institute of Technology, Shanghai 201418, ChinaSpice and Beverage Research Institute, Chinese Academy of Tropical Agriculture Science, Wanning 571533, ChinaSpice and Beverage Research Institute, Chinese Academy of Tropical Agriculture Science, Wanning 571533, ChinaSpice and Beverage Research Institute, Chinese Academy of Tropical Agriculture Science, Wanning 571533, ChinaNujiang Green Spice Industry Research Institute, Nujiang 673200, ChinaNujiang Green Spice Industry Research Institute, Nujiang 673200, ChinaNujiang Prefecture Rural Science and Technology Productivity Promotion Center, Nujiang 673200, ChinaNujiang Prefecture Rural Science and Technology Productivity Promotion Center, Nujiang 673200, ChinaSchool of Ecological Technology and Engineering, Shanghai Institute of Technology, Shanghai 201418, ChinaSpice and Beverage Research Institute, Chinese Academy of Tropical Agriculture Science, Wanning 571533, ChinaIn order to obtain the best extraction process of smoked Amomum tsaoko(SDAT) oleoresin, the extraction solvent, extraction temperature, solid-liquid ratio, extraction time and particle size were regarded as the influence factors. On the basis of single factor experiment, the eexperimental design of three factors and three levels was used by Box-Benhnken central composite method, according to the extraction rate of SDAT oleoresin as the response value, and the extraction conditions were further optimized by response surface methodology(RSM). The results showed that the optimum process conditions of SDAT oleoresin was as follows: Anhydrous methanol as solvent, extraction temperature was 75 ℃, solid-liquidratio was 1:20(g/mL), extraction time was 7 h and particle size was 80 mesh. The regression equation predicted that the theoretical extraction rate of SDAT could reach 9.57%, the average extraction rate of the three validation experiments was 9.48%, and the predicted value was close to the actual result. And 58 compounds were identified by GC-TOF-MS, including alcohols(31.59%), aldehydes(21.13%), alkenes(1.23%), ketones(1.56%), esters(2.38%) and phenols(0.79%), 1,8-eucalyptol(9.28%), α-terpineol(3.55%), gera-niol(8.4%), trans citral(5.78%), 2-methyl-3-ph-enylpropanal(6.33%), etc. Through the determination of the best process of SDAT oleoresin, the detected components are mainly concentrated in alcohols and aldehydes, which provides a theoretical basis for the nutritional components and biological activity of grass fruit oleoresin in the later stage.http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2021040002smoked amomum tsaokoheating reflux methodresponse surface methodgc-tof-mscomponent analysis |
| spellingShingle | Yi LIN Mei HUANG Guiping WU Fei XU Juncai HE Shengjun YOU Penghui GAO Linna LIU Meifang HOU Fenglin GU Optimization of Extraction Process and Component Analysis of Oleoresin from Smoked Amomum tsaoko by Response Surface Methodology Shipin gongye ke-ji smoked amomum tsaoko heating reflux method response surface method gc-tof-ms component analysis |
| title | Optimization of Extraction Process and Component Analysis of Oleoresin from Smoked Amomum tsaoko by Response Surface Methodology |
| title_full | Optimization of Extraction Process and Component Analysis of Oleoresin from Smoked Amomum tsaoko by Response Surface Methodology |
| title_fullStr | Optimization of Extraction Process and Component Analysis of Oleoresin from Smoked Amomum tsaoko by Response Surface Methodology |
| title_full_unstemmed | Optimization of Extraction Process and Component Analysis of Oleoresin from Smoked Amomum tsaoko by Response Surface Methodology |
| title_short | Optimization of Extraction Process and Component Analysis of Oleoresin from Smoked Amomum tsaoko by Response Surface Methodology |
| title_sort | optimization of extraction process and component analysis of oleoresin from smoked amomum tsaoko by response surface methodology |
| topic | smoked amomum tsaoko heating reflux method response surface method gc-tof-ms component analysis |
| url | http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2021040002 |
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