Syntheses, crystal structures and Hirshfeld surface analysis of 2-(benzylsulfanyl)-5-[4-(dimethylamino)phenyl]-1,3,4-oxadiazole and 2-[(2-chloro-6-fluorobenzyl)sulfanyl]-5-[4-(dimethylamino)phenyl]-1,3,4-oxadiazole

Syntheses, crystal structures and Hirshfeld surface analysis of 2-(benzylsulfanyl)-5-[4-(dimethylamino)phenyl]-1,3,4-oxadiazole and 2-[(2-chloro-6-fluorobenzyl)sulfanyl]-5-[4-(dimethylamino)phenyl]-1,3,4-oxadiazole

The title compounds were synthesized by alkylation of 5-[(4-dimethylamino)phenyl]-1,3,4-oxadiazole-2-thiol with benzyl chloride or 2-chloro-6-fluorobenzyl chloride in the presence of potassium carbonate. The yields of 2-(benzylsulfanyl)-5-[4-(dimethylamino)phenyl]-1,3,4-oxadiazole, C17H17N3OS (I), a...

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Bibliographic Details
Main Authors: Rasul Ya. Okmanov, Abdukhakim A. Ziyaev, Azimboy Sh. Abdukarimov, Turdibek T. Toshmurodov, Tursunali S. Kholikov
Format: Article
Language:English
Published: International Union of Crystallography 2023-06-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
synthesis
1,3,4-oxadiazole
crystal structure
hirshfeld surface analysis
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989023004164

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http://scripts.iucr.org/cgi-bin/paper?S2056989023004164

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