Tetrapropylammonium Occlusion in Nanoaggregates of Precursor of Silicalite-1 Zeolite Studied by 1H and 13C NMR

The dynamic behavior of tetrapropylammonium (TPA) cations in the clear precursor sols for silicalite synthesis has been investigated by 1H diffusion ordered spectroscopy (DOSY), T1, T2, and T1ρ 1H relaxation, as well as 1H→13C cross polarization (CP) nuclear magnetic resonance. The DOSY NMR experime...

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Bibliographic Details
Main Authors: Mohamed Haouas, David P. Petry, Michael W. Anderson, Francis Taulelle
Format: Article
Language:English
Published: MDPI AG 2016-06-01
Series:Inorganics
Subjects:
Online Access:http://www.mdpi.com/2304-6740/4/2/18