Crystal structure of diethylammonium dioxido{Z)-N-[(pyridin-2-yl)carbonylazanidyl]pyridine-2-carboximidato}vanadate(1−) monohydrate

Crystal structure of diethylammonium dioxido{Z)-N-[(pyridin-2-yl)carbonylazanidyl]pyridine-2-carboximidato}vanadate(1−) monohydrate

The title compound, (C4H12N)[V(C12H8N4O2)O2]·H2O, was synthesized via aerial oxidation on refluxing picolinohydrazide with ethyl picolinate followed by addition of VIVO(acac)2 and diethylamine in methanol. It crystallizes in the triclinic crystal system in space group P\overline{1}. In the complex a...

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Bibliographic Details
Main Author: Bipul Mondal
Format: Article
Language:English
Published: International Union of Crystallography 2024-03-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
dioxidovanadium(v)
o,n,o -donor schiff-base
hydrogen bond
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989024001166

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http://scripts.iucr.org/cgi-bin/paper?S2056989024001166

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