Study of Some Properties of PbI2 Deposited on Porous Silicon Using Thermal Evaporation Technique for Many Applications

The present work is a study of some properties of PbI<sub>2</sub> deposited on porous silicon (n-PSi) by using the thermal evaporation technique. X-ray diffraction, scanning electron microscopy, UV–Vis spectrophotometer, and FTIR analysis were used to characterize the structural, optical...

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Main Authors: Suha Ali, Mohammed Mohammed, Fatima Sultan
Format: Article
Language:English
Published: University of Technology, Baghdad 2022-09-01
Series:Journal of Applied Sciences and Nanotechnology
Subjects:
Online Access:https://jasn.uotechnology.edu.iq/article_19437_f4c3b1b54ca0e0c568e546618fd12c1c.pdf
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author Suha Ali
Mohammed Mohammed
Fatima Sultan
author_facet Suha Ali
Mohammed Mohammed
Fatima Sultan
author_sort Suha Ali
collection DOAJ
description The present work is a study of some properties of PbI<sub>2</sub> deposited on porous silicon (n-PSi) by using the thermal evaporation technique. X-ray diffraction, scanning electron microscopy, UV–Vis spectrophotometer, and FTIR analysis were used to characterize the structural, optical, and morphological properties of n-Psi. X-ray diffraction showed that the PbI<sub>2</sub> film has a hexagonal polycrystalline structure, while FE-SEM images showed porous silicone in Photoelectrochemical etching, the pore distribution is irregular and the pore refers to the increased surface area of the silicon. SEM images of pbI<sub>2</sub> film showed that particles were scattered and resembled gravel in size. The estimated optical energy value of thin films of PbI<sub>2</sub> was 2.6 eV. PbI<sub>2</sub> film has lower transmittance values at short wavelengths, but as the wavelength increases, the transmittance values gradually increased. The greatest transmittance value was 0.88. From FTIR analysis, chemical bonds were determined between porous silicon and PbI<sub>2</sub>.
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spelling doaj.art-62876bc3adfd4e058f926dd4a2510f332022-12-22T03:19:51ZengUniversity of Technology, BaghdadJournal of Applied Sciences and Nanotechnology2788-68672022-09-012315716510.53293/jasn.2022.4563.112619437Study of Some Properties of PbI2 Deposited on Porous Silicon Using Thermal Evaporation Technique for Many ApplicationsSuha Ali0Mohammed Mohammed1Fatima Sultan2Department of Applied Sciences, University of Technology – IraqDepartment of Applied Sciences, University of Technology – IraqDepartment of Applied Sciences, University of Technology – IraqThe present work is a study of some properties of PbI<sub>2</sub> deposited on porous silicon (n-PSi) by using the thermal evaporation technique. X-ray diffraction, scanning electron microscopy, UV–Vis spectrophotometer, and FTIR analysis were used to characterize the structural, optical, and morphological properties of n-Psi. X-ray diffraction showed that the PbI<sub>2</sub> film has a hexagonal polycrystalline structure, while FE-SEM images showed porous silicone in Photoelectrochemical etching, the pore distribution is irregular and the pore refers to the increased surface area of the silicon. SEM images of pbI<sub>2</sub> film showed that particles were scattered and resembled gravel in size. The estimated optical energy value of thin films of PbI<sub>2</sub> was 2.6 eV. PbI<sub>2</sub> film has lower transmittance values at short wavelengths, but as the wavelength increases, the transmittance values gradually increased. The greatest transmittance value was 0.88. From FTIR analysis, chemical bonds were determined between porous silicon and PbI<sub>2</sub>.https://jasn.uotechnology.edu.iq/article_19437_f4c3b1b54ca0e0c568e546618fd12c1c.pdflead iodideporous siliconthermal evaporationx-ray diffraction
spellingShingle Suha Ali
Mohammed Mohammed
Fatima Sultan
Study of Some Properties of PbI2 Deposited on Porous Silicon Using Thermal Evaporation Technique for Many Applications
Journal of Applied Sciences and Nanotechnology
lead iodide
porous silicon
thermal evaporation
x-ray diffraction
title Study of Some Properties of PbI2 Deposited on Porous Silicon Using Thermal Evaporation Technique for Many Applications
title_full Study of Some Properties of PbI2 Deposited on Porous Silicon Using Thermal Evaporation Technique for Many Applications
title_fullStr Study of Some Properties of PbI2 Deposited on Porous Silicon Using Thermal Evaporation Technique for Many Applications
title_full_unstemmed Study of Some Properties of PbI2 Deposited on Porous Silicon Using Thermal Evaporation Technique for Many Applications
title_short Study of Some Properties of PbI2 Deposited on Porous Silicon Using Thermal Evaporation Technique for Many Applications
title_sort study of some properties of pbi2 deposited on porous silicon using thermal evaporation technique for many applications
topic lead iodide
porous silicon
thermal evaporation
x-ray diffraction
url https://jasn.uotechnology.edu.iq/article_19437_f4c3b1b54ca0e0c568e546618fd12c1c.pdf
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AT fatimasultan studyofsomepropertiesofpbi2depositedonporoussiliconusingthermalevaporationtechniqueformanyapplications