Development of an HPLC method with relative molar sensitivity based on 1H-qNMR to determine acteoside and pedaliin in dried sesame leaf powders and processed foods.

A high-performance liquid chromatography (HPLC) method with relative molar sensitivity (RMS) based on 1H quantitative NMR spectroscopy (1H-qNMR) has been developed for food ingredients such as acteoside (verbascoside) and pedaliin (pedalitin-6-O-glucoside) without requiring authentic and identical s...

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Bibliographic Details
Main Authors: Takashi Ohtsuki, Kiyoaki Matsuoka, Yushiro Fuji, Yuzo Nishizaki, Naoko Masumoto, Naoki Sugimoto, Kyoko Sato, Hiroshi Matsufuji
Format: Article
Language:English
Published: Public Library of Science (PLoS) 2020-01-01
Series:PLoS ONE
Online Access:https://doi.org/10.1371/journal.pone.0243175