One-Pot Synthesis and Crystal Structure of Methyl 5-Hydroxy-1-phenyl-1H-pyrazole-3-carboxylate

The title compound, Methyl 5-Hydroxy-1-Phenyl-1H-Pyrazole-3-Carboxylate (C11H10N2O3), was prepared by a one-pot, two-component reaction of an equimolar mixture of phenyl hydrazine and dimethyl acetylene dicarboxylate (DMAD) at reflux temperature for 2 h in a mixture of toluene and dichloromethane as...

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Bibliographic Details
Main Authors: Aamer Saeed, Ifzan Arshad, Ulrich Flörke
Format: Article
Language:English
Published: MDPI AG 2012-08-01
Series:Crystals
Subjects:
Online Access:http://www.mdpi.com/2073-4352/2/3/1248