Pentafluoropropionic Anhydride Derivatization and GC-MS Analysis of Histamine, Agmatine, Putrescine, and Spermidine: Effects of Solvents and Starting Column Temperature

Pentafluoropropionic Anhydride Derivatization and GC-MS Analysis of Histamine, Agmatine, Putrescine, and Spermidine: Effects of Solvents and Starting Column Temperature

Gas chromatography–mass spectrometry (GC-MS) is useful for the quantitative determination of the polyamines spermidine (SPD) and putrescine (PUT) and of the biogenic amine agmatine (AGM) in biological samples after derivatization. This GC-MS method involves a two-step extraction with <i>n</...

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Bibliographic Details
Main Authors: Dimitrios Tsikas, Bibiana Beckmann, Svetlana Baskal, Gorig Brunner
Format: Article
Language:English
Published: MDPI AG 2023-01-01
Series:Molecules
Subjects:
acylation
amidation
amines
biogenic amines
derivatization
GC-MS
Online Access:https://www.mdpi.com/1420-3049/28/3/939

Internet

https://www.mdpi.com/1420-3049/28/3/939

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