Comparison of Anodic and Au-Au Thermocompression Si-Wafer Bonding Methods for High-Pressure Microcooling Devices

Silicon-based microchannel technology offers unmatched performance in the cooling of silicon pixel detectors in high-energy physics. Although Si–Si direct bonding, used for the fabrication of cooling plates, also meets the stringent requirements of this application (its high-pressure resistance of ~...

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Main Authors: Sylwester Bargiel, Julien Cogan, Samuel Queste, Stefania Oliveri, Ludovic Gauthier-Manuel, Marina Raschetti, Olivier Leroy, Stéphan Beurthey, Mathieu Perrin-Terrin
Format: Article
Language:English
Published: MDPI AG 2023-06-01
Series:Micromachines
Subjects:
Online Access:https://www.mdpi.com/2072-666X/14/7/1297
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author Sylwester Bargiel
Julien Cogan
Samuel Queste
Stefania Oliveri
Ludovic Gauthier-Manuel
Marina Raschetti
Olivier Leroy
Stéphan Beurthey
Mathieu Perrin-Terrin
author_facet Sylwester Bargiel
Julien Cogan
Samuel Queste
Stefania Oliveri
Ludovic Gauthier-Manuel
Marina Raschetti
Olivier Leroy
Stéphan Beurthey
Mathieu Perrin-Terrin
author_sort Sylwester Bargiel
collection DOAJ
description Silicon-based microchannel technology offers unmatched performance in the cooling of silicon pixel detectors in high-energy physics. Although Si–Si direct bonding, used for the fabrication of cooling plates, also meets the stringent requirements of this application (its high-pressure resistance of ~200 bar, in particular), its use is reported to be a challenging and expensive process. In this study, we evaluated two alternative bonding methods, aiming toward a more cost-effective fabrication process: Si-Glass-Si anodic bonding (AB) with a thin-film glass, and Au-Au thermocompression (TC). The bonding strengths of the two methods were evaluated with destructive pressure burst tests (0–690 bar) on test structures, each made of a 1 × 2 cm<sup>2</sup> silicon die etched with a tank and an inlet channel and sealed with a plain silicon die using either the AB or TC bonding. The pressure resistance of the structures was measured to be higher for the TC-sealed samples (max. 690 bar) than for the AB samples (max. 530 bar), but less homogeneous. The failure analysis indicated that the AB structure resistance was limited by the adhesion force of the deposited layers. Nevertheless, both the TC and AB methods provided sufficient bond quality to hold the high pressure required for application in high-energy physics pixel detector cooling.
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spelling doaj.art-78d5f37d0acb4741b25282be3576b01a2023-11-18T20:31:26ZengMDPI AGMicromachines2072-666X2023-06-01147129710.3390/mi14071297Comparison of Anodic and Au-Au Thermocompression Si-Wafer Bonding Methods for High-Pressure Microcooling DevicesSylwester Bargiel0Julien Cogan1Samuel Queste2Stefania Oliveri3Ludovic Gauthier-Manuel4Marina Raschetti5Olivier Leroy6Stéphan Beurthey7Mathieu Perrin-Terrin8Institut FEMTO-ST, CNRS, Université de Franche-Comté, F-25000 Besançon, FranceAix Marseille University, CNRS/IN2P3, CPPM, Marseille, FranceInstitut FEMTO-ST, CNRS, Université de Franche-Comté, F-25000 Besançon, FranceInstitut FEMTO-ST, CNRS, Université de Franche-Comté, F-25000 Besançon, FranceInstitut FEMTO-ST, CNRS, Université de Franche-Comté, F-25000 Besançon, FranceInstitut FEMTO-ST, CNRS, Université de Franche-Comté, F-25000 Besançon, FranceAix Marseille University, CNRS/IN2P3, CPPM, Marseille, FranceAix Marseille University, CNRS/IN2P3, CPPM, Marseille, FranceAix Marseille University, CNRS/IN2P3, CPPM, Marseille, FranceSilicon-based microchannel technology offers unmatched performance in the cooling of silicon pixel detectors in high-energy physics. Although Si–Si direct bonding, used for the fabrication of cooling plates, also meets the stringent requirements of this application (its high-pressure resistance of ~200 bar, in particular), its use is reported to be a challenging and expensive process. In this study, we evaluated two alternative bonding methods, aiming toward a more cost-effective fabrication process: Si-Glass-Si anodic bonding (AB) with a thin-film glass, and Au-Au thermocompression (TC). The bonding strengths of the two methods were evaluated with destructive pressure burst tests (0–690 bar) on test structures, each made of a 1 × 2 cm<sup>2</sup> silicon die etched with a tank and an inlet channel and sealed with a plain silicon die using either the AB or TC bonding. The pressure resistance of the structures was measured to be higher for the TC-sealed samples (max. 690 bar) than for the AB samples (max. 530 bar), but less homogeneous. The failure analysis indicated that the AB structure resistance was limited by the adhesion force of the deposited layers. Nevertheless, both the TC and AB methods provided sufficient bond quality to hold the high pressure required for application in high-energy physics pixel detector cooling.https://www.mdpi.com/2072-666X/14/7/1297bonding technologyanodic bondingthermocompression bondingmicrocoolingmicrofluidic deviceburst pressure test
spellingShingle Sylwester Bargiel
Julien Cogan
Samuel Queste
Stefania Oliveri
Ludovic Gauthier-Manuel
Marina Raschetti
Olivier Leroy
Stéphan Beurthey
Mathieu Perrin-Terrin
Comparison of Anodic and Au-Au Thermocompression Si-Wafer Bonding Methods for High-Pressure Microcooling Devices
Micromachines
bonding technology
anodic bonding
thermocompression bonding
microcooling
microfluidic device
burst pressure test
title Comparison of Anodic and Au-Au Thermocompression Si-Wafer Bonding Methods for High-Pressure Microcooling Devices
title_full Comparison of Anodic and Au-Au Thermocompression Si-Wafer Bonding Methods for High-Pressure Microcooling Devices
title_fullStr Comparison of Anodic and Au-Au Thermocompression Si-Wafer Bonding Methods for High-Pressure Microcooling Devices
title_full_unstemmed Comparison of Anodic and Au-Au Thermocompression Si-Wafer Bonding Methods for High-Pressure Microcooling Devices
title_short Comparison of Anodic and Au-Au Thermocompression Si-Wafer Bonding Methods for High-Pressure Microcooling Devices
title_sort comparison of anodic and au au thermocompression si wafer bonding methods for high pressure microcooling devices
topic bonding technology
anodic bonding
thermocompression bonding
microcooling
microfluidic device
burst pressure test
url https://www.mdpi.com/2072-666X/14/7/1297
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