Implementation of Cloud Point Extraction Using Surfactants in the Recovery of Polyphenols from Apricot Cannery Waste

The objective of this study was to investigate the feasibility of using Cloud Point Extraction (CPE) to isolate natural antioxidants (polyphenols) from apricot cannery waste (ACW). Four different food-grade surfactants (Genapol X-080, PEG 8000, Tween 80, and Lecithin) were tested at varying concentr...

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Main Authors: Ioannis Giovanoudis, Vassilis Athanasiadis, Theodoros Chatzimitakos, Dimitrios Kalompatsios, Eleni Bozinou, Olga Gortzi, George D. Nanos, Stavros I. Lalas
Format: Article
Language:English
Published: MDPI AG 2023-04-01
Series:Eng
Subjects:
Online Access:https://www.mdpi.com/2673-4117/4/2/72
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author Ioannis Giovanoudis
Vassilis Athanasiadis
Theodoros Chatzimitakos
Dimitrios Kalompatsios
Eleni Bozinou
Olga Gortzi
George D. Nanos
Stavros I. Lalas
author_facet Ioannis Giovanoudis
Vassilis Athanasiadis
Theodoros Chatzimitakos
Dimitrios Kalompatsios
Eleni Bozinou
Olga Gortzi
George D. Nanos
Stavros I. Lalas
author_sort Ioannis Giovanoudis
collection DOAJ
description The objective of this study was to investigate the feasibility of using Cloud Point Extraction (CPE) to isolate natural antioxidants (polyphenols) from apricot cannery waste (ACW). Four different food-grade surfactants (Genapol X-080, PEG 8000, Tween 80, and Lecithin) were tested at varying concentrations to evaluate the effectiveness of the technique. It was observed that low concentrations of surfactants in one-step CPE resulted in less than 65% polyphenol recovery, which necessitated further extraction steps. However, high concentrations of surfactants were found to significantly improve polyphenol extraction from ACW for all surfactants tested. Among the four surfactants, PEG 8000 was found to be the most effective in most circumstances; specifically, adding only 2% of the surfactant per step in a two-step CPE was enough to effectively extract polyphenols with recovery rates better than 99%. When 10% <i>w</i>/<i>v</i> of PEG 8000 was used, recoveries greater than 92% were obtained. Since PEG 8000 is a reagent with low toxicity and the CPE method is simple, rapid, cheap, sensitive, and selective, the extracted organic compounds from ACW can be used as natural antioxidants in food technology. This has important implications for the development of natural and sustainable food additives.
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spelling doaj.art-8310a4a9caec4af48a3aaea09104bda02023-11-18T10:14:57ZengMDPI AGEng2673-41172023-04-01421225123510.3390/eng4020072Implementation of Cloud Point Extraction Using Surfactants in the Recovery of Polyphenols from Apricot Cannery WasteIoannis Giovanoudis0Vassilis Athanasiadis1Theodoros Chatzimitakos2Dimitrios Kalompatsios3Eleni Bozinou4Olga Gortzi5George D. Nanos6Stavros I. Lalas7Department of Food Science and Nutrition, University of Thessaly, Terma N. Temponera Street, 43100 Karditsa, GreeceDepartment of Food Science and Nutrition, University of Thessaly, Terma N. Temponera Street, 43100 Karditsa, GreeceDepartment of Food Science and Nutrition, University of Thessaly, Terma N. Temponera Street, 43100 Karditsa, GreeceDepartment of Food Science and Nutrition, University of Thessaly, Terma N. Temponera Street, 43100 Karditsa, GreeceDepartment of Food Science and Nutrition, University of Thessaly, Terma N. Temponera Street, 43100 Karditsa, GreeceDepartment of Agriculture Crop Production and Rural Environment, School of Agricultural Sciences, University of Thessaly, 38446 Volos, GreeceDepartment of Agriculture Crop Production and Rural Environment, School of Agricultural Sciences, University of Thessaly, 38446 Volos, GreeceDepartment of Food Science and Nutrition, University of Thessaly, Terma N. Temponera Street, 43100 Karditsa, GreeceThe objective of this study was to investigate the feasibility of using Cloud Point Extraction (CPE) to isolate natural antioxidants (polyphenols) from apricot cannery waste (ACW). Four different food-grade surfactants (Genapol X-080, PEG 8000, Tween 80, and Lecithin) were tested at varying concentrations to evaluate the effectiveness of the technique. It was observed that low concentrations of surfactants in one-step CPE resulted in less than 65% polyphenol recovery, which necessitated further extraction steps. However, high concentrations of surfactants were found to significantly improve polyphenol extraction from ACW for all surfactants tested. Among the four surfactants, PEG 8000 was found to be the most effective in most circumstances; specifically, adding only 2% of the surfactant per step in a two-step CPE was enough to effectively extract polyphenols with recovery rates better than 99%. When 10% <i>w</i>/<i>v</i> of PEG 8000 was used, recoveries greater than 92% were obtained. Since PEG 8000 is a reagent with low toxicity and the CPE method is simple, rapid, cheap, sensitive, and selective, the extracted organic compounds from ACW can be used as natural antioxidants in food technology. This has important implications for the development of natural and sustainable food additives.https://www.mdpi.com/2673-4117/4/2/72cloud point extractionpolyphenolssurfactantsapricot cannery wastefood industry
spellingShingle Ioannis Giovanoudis
Vassilis Athanasiadis
Theodoros Chatzimitakos
Dimitrios Kalompatsios
Eleni Bozinou
Olga Gortzi
George D. Nanos
Stavros I. Lalas
Implementation of Cloud Point Extraction Using Surfactants in the Recovery of Polyphenols from Apricot Cannery Waste
Eng
cloud point extraction
polyphenols
surfactants
apricot cannery waste
food industry
title Implementation of Cloud Point Extraction Using Surfactants in the Recovery of Polyphenols from Apricot Cannery Waste
title_full Implementation of Cloud Point Extraction Using Surfactants in the Recovery of Polyphenols from Apricot Cannery Waste
title_fullStr Implementation of Cloud Point Extraction Using Surfactants in the Recovery of Polyphenols from Apricot Cannery Waste
title_full_unstemmed Implementation of Cloud Point Extraction Using Surfactants in the Recovery of Polyphenols from Apricot Cannery Waste
title_short Implementation of Cloud Point Extraction Using Surfactants in the Recovery of Polyphenols from Apricot Cannery Waste
title_sort implementation of cloud point extraction using surfactants in the recovery of polyphenols from apricot cannery waste
topic cloud point extraction
polyphenols
surfactants
apricot cannery waste
food industry
url https://www.mdpi.com/2673-4117/4/2/72
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