Research of selective etching in LiNbO3 using proton-exchanged wet etching technique

Lithium niobate material (LN) has shown great application potentials in the fabrication of integrated optical devices due to its excellent physical properties, especially with the occurrence of lithium niobate-on-insulator (LNOI) substrate. However, the greatest challenge of micro/nano optical devic...

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Main Authors: Ying Li, Tian Lan, Dengcai Yang, Meihua Xiang, Jingjing Dai, Chong Li, Zhiyong Wang
Format: Article
Language:English
Published: IOP Publishing 2020-01-01
Series:Materials Research Express
Subjects:
Online Access:https://doi.org/10.1088/2053-1591/ab8e70
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author Ying Li
Tian Lan
Dengcai Yang
Meihua Xiang
Jingjing Dai
Chong Li
Zhiyong Wang
author_facet Ying Li
Tian Lan
Dengcai Yang
Meihua Xiang
Jingjing Dai
Chong Li
Zhiyong Wang
author_sort Ying Li
collection DOAJ
description Lithium niobate material (LN) has shown great application potentials in the fabrication of integrated optical devices due to its excellent physical properties, especially with the occurrence of lithium niobate-on-insulator (LNOI) substrate. However, the greatest challenge of micro/nano optical devices based on LN material lies in the precise etching process and thus limits its applications. In this paper, we comprehensively analyze the etching results treated by the proposed proton-exchanged wet-etching method (PEWE) combining with theoretical simulations and experiments. It is found that the proton-exchanged layer in the LN material can be easily etched after using a mixture acid of HF/HNO _3 , leading to the improvement of etching rate and surface morphology. The lowest roughness of the optical waveguide is measured to be 0.81 nm, which is beneficial for the performance improvement of LN-based optical devices. Ultimately, a quasi-vertical sidewall of the upper part of optical waveguide with improved surface morphology is successfully realized by utilizing the PEWE. Moreover, this method could also be extended to improve the performance of LNOI-based optical devices and pave the way for ultra-compact photonic integrated circuits based on LNOI.
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spelling doaj.art-8c557d38e3d6460691af223eca5e2f602023-08-09T16:10:53ZengIOP PublishingMaterials Research Express2053-15912020-01-017505620210.1088/2053-1591/ab8e70Research of selective etching in LiNbO3 using proton-exchanged wet etching techniqueYing Li0https://orcid.org/0000-0003-1696-7569Tian Lan1https://orcid.org/0000-0003-3549-2255Dengcai Yang2Meihua Xiang3Jingjing Dai4Chong Li5Zhiyong Wang6https://orcid.org/0000-0002-8751-9432Institute of Advanced Technology on Semiconductor Optics &Electronics, Institute of Laser Engineering, Beijing University of Technology , Beijing, 100124, People’s Republic of ChinaInstitute of Advanced Technology on Semiconductor Optics &Electronics, Institute of Laser Engineering, Beijing University of Technology , Beijing, 100124, People’s Republic of ChinaInstitute of Advanced Technology on Semiconductor Optics &Electronics, Institute of Laser Engineering, Beijing University of Technology , Beijing, 100124, People’s Republic of ChinaInstitute of Advanced Technology on Semiconductor Optics &Electronics, Institute of Laser Engineering, Beijing University of Technology , Beijing, 100124, People’s Republic of ChinaInstitute of Advanced Technology on Semiconductor Optics &Electronics, Institute of Laser Engineering, Beijing University of Technology , Beijing, 100124, People’s Republic of ChinaCollege of Microelectronics, Beijing University of technology , Beijing 100124, People’s Republic of ChinaInstitute of Advanced Technology on Semiconductor Optics &Electronics, Institute of Laser Engineering, Beijing University of Technology , Beijing, 100124, People’s Republic of ChinaLithium niobate material (LN) has shown great application potentials in the fabrication of integrated optical devices due to its excellent physical properties, especially with the occurrence of lithium niobate-on-insulator (LNOI) substrate. However, the greatest challenge of micro/nano optical devices based on LN material lies in the precise etching process and thus limits its applications. In this paper, we comprehensively analyze the etching results treated by the proposed proton-exchanged wet-etching method (PEWE) combining with theoretical simulations and experiments. It is found that the proton-exchanged layer in the LN material can be easily etched after using a mixture acid of HF/HNO _3 , leading to the improvement of etching rate and surface morphology. The lowest roughness of the optical waveguide is measured to be 0.81 nm, which is beneficial for the performance improvement of LN-based optical devices. Ultimately, a quasi-vertical sidewall of the upper part of optical waveguide with improved surface morphology is successfully realized by utilizing the PEWE. Moreover, this method could also be extended to improve the performance of LNOI-based optical devices and pave the way for ultra-compact photonic integrated circuits based on LNOI.https://doi.org/10.1088/2053-1591/ab8e70lithium niobate (LN)optical waveguideproton exchange (PE)wet etching
spellingShingle Ying Li
Tian Lan
Dengcai Yang
Meihua Xiang
Jingjing Dai
Chong Li
Zhiyong Wang
Research of selective etching in LiNbO3 using proton-exchanged wet etching technique
Materials Research Express
lithium niobate (LN)
optical waveguide
proton exchange (PE)
wet etching
title Research of selective etching in LiNbO3 using proton-exchanged wet etching technique
title_full Research of selective etching in LiNbO3 using proton-exchanged wet etching technique
title_fullStr Research of selective etching in LiNbO3 using proton-exchanged wet etching technique
title_full_unstemmed Research of selective etching in LiNbO3 using proton-exchanged wet etching technique
title_short Research of selective etching in LiNbO3 using proton-exchanged wet etching technique
title_sort research of selective etching in linbo3 using proton exchanged wet etching technique
topic lithium niobate (LN)
optical waveguide
proton exchange (PE)
wet etching
url https://doi.org/10.1088/2053-1591/ab8e70
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