SPME-GC-MS测定‘凤丹’牡丹籽油挥发物组成时固相微萃取条件的响应面优化Response surface optimization of solid phase microextraction condition for the determination of volatiles in Fengdan seed oil by SPME-GC-MS

SPME-GC-MS测定‘凤丹’牡丹籽油挥发物组成时固相微萃取条件的响应面优化Response surface optimization of solid phase microextraction condition for the determination of volatiles in Fengdan seed oil by SPME-GC-MS

为‘凤丹’牡丹籽油风味研究提供参考，采用固相微萃取技术结合气相色谱-质谱法（SPME-GC-MS）测定‘凤丹’牡丹籽油挥发物组成。在单因素试验基础上，根据Box-Behnken试验设计原理，以‘凤丹’牡丹籽油挥发物总峰面积为响应值，以样品量、平衡时间、萃取时间、萃取温度为因素进行响应面试验，对‘凤丹’牡丹籽油挥发物的固相微萃取条件进行优化，然后采用SPME-GC-MS测定‘凤丹’牡丹籽油的挥发物组成及相对含量。结果表明：固相微萃取‘凤丹’牡丹籽油挥发物的最佳条件为样品量4.0 g（15 mL样品瓶），平衡时间40 min，萃取时间20 min，萃取温度80 ℃；在最佳条件下结合GC-MS分析测...

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Bibliographic Details
Main Author: 帅佳琪1，吕长平2,3，秧拯民1，石杨1，毛咪1，江莉娜1，康敏1 SHUAI Jiaqi1, LYU Changping2,3, YANG Zhengmin1, SHI Yang1, MAO Mi1, JIANG Lina1, KANG Min1
Format: Article
Language:English
Published: 中粮工科（西安）国际工程有限公司 2023-04-01
Series:Zhongguo youzhi
Subjects:
‘凤丹’牡丹籽油；挥发物；固相微萃取；响应面优化；气相色谱-质谱法
fengdan seed oil; volatile; solid phase microextraction; response surface optimization; gas chromatography-mass spectrometry
Online Access:http://tg.chinaoils.cn/ch/reader/create_pdf.aspx?file_no=20230411&year_id=2023&quarter_id=4&falg=1

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http://tg.chinaoils.cn/ch/reader/create_pdf.aspx?file_no=20230411&year_id=2023&quarter_id=4&falg=1

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