To establish a method for the determination of phthalic acid esters in Peanut oil, Peanut oil samples were extracted with n-hexane saturated acetonitrile, purified by 25 mg PSA and 25 mg C18 and detected by GC-MS selected ion monitoring (SIM) mode detection, external standard method quantitative.The standard solution of 17 phthalates showed a good linearity in the concentration range of 0.02～3.0 mg/L,and the correlation coefficient (r) is above 0.999, the detection limit (LOD) was 0.01 mg/kg to 0.02 mg/kg,and the quantitative limit (LQD) was 0.03 mg/kg to 0.05 mg/kg. the recovery of standard addition was 92.47% to 108.72%, and the relative standard deviation was 1.10% to 5.94%.The method is simple, rapid,sensitive and accurate. and can be used for the determination of 17 phthalates in Peanut oils.

To establish a method for the determination of phthalic acid esters in Peanut oil, Peanut oil samples were extracted with n-hexane saturated acetonitrile, purified by 25 mg PSA and 25 mg C18 and detected by GC-MS selected ion monitoring (SIM) mode detection, external standard method quantitative.The standard solution of 17 phthalates showed a good linearity in the concentration range of 0.02～3.0 mg/L,and the correlation coefficient (r) is above 0.999, the detection limit (LOD) was 0.01 mg/kg to 0.02 mg/kg,and the quantitative limit (LQD) was 0.03 mg/kg to 0.05 mg/kg. the recovery of standard addition was 92.47% to 108.72%, and the relative standard deviation was 1.10% to 5.94%.The method is simple, rapid,sensitive and accurate. and can be used for the determination of 17 phthalates in Peanut oils.

To establish a method for the determination of phthalic acid esters in Peanut oil, Peanut oil samples were extracted with n-hexane saturated acetonitrile, purified by 25 mg PSA and 25 mg C18 and detected by GC-MS selected ion monitoring (SIM) mode detection, external standard method quantitative.Th...

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Bibliographic Details
Main Authors: GAO Xia, CHEN Hui, LI Yu-xiu, LI Wen-jun, TAN Min
Format: Article
Language:English
Published: Academy of National Food and Strategic Reserves Administration 2020-09-01
Series:Liang you shipin ke-ji
Subjects:
quechers
gas chromatography-mass spectrometry (gc/ms)
peanut oils
phthalates
Online Access:http://lyspkj.ijournal.cn/lyspkj/article/abstract/20200525?st=article_issue

Internet

http://lyspkj.ijournal.cn/lyspkj/article/abstract/20200525?st=article_issue

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