Crystal structure of {2,2′-[ethylenebis(nitrilomethanylylidene)]diphenolato-κ4O,N,N′,O′}oxidovanadium(IV) methanol monosolvate

Crystal structure of {2,2′-[ethylenebis(nitrilomethanylylidene)]diphenolato-κ4O,N,N′,O′}oxidovanadium(IV) methanol monosolvate

Two independent molecules of the title solvated complex, [V(C16H14N2O2)O]·CH3OH, also known as [N,N′-bis(salicylidene)ethylenediamine]oxidovanadium(IV) or vanadyl salen, crystallize in the asymmetric unit. Each disordered methanol solvent molecule [occupancy ratios 0.678 (4):0.322 (4) and 0.750 (5):...

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Bibliographic Details
Main Authors: Rachel E. Hsuan, Jemma E. Hughes, Thomas H. Miller, Nabila Shaikh, Phoebe H. M. Cunningham, Alice E. O'Connor, Jeremiah P. Tidey, Alexander J. Blake
Format: Article
Language:English
Published: International Union of Crystallography 2014-11-01
Series:Acta Crystallographica Section E
Subjects:
crystal structure
oxidovanadium(IV)
2,2′-[ethylenebis(nitrilomethanylylidene)]diphenolate
N,N′-bis(salicylidene)ethylenediamine
hydrogen bonding
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536814023332

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http://scripts.iucr.org/cgi-bin/paper?S1600536814023332

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