In situ/operando plug-flow fixed-bed cell for synchrotron PXRD and XAFS investigations at high temperature, pressure, controlled gas atmosphere and ultra-fast heating

In situ/operando plug-flow fixed-bed cell for synchrotron PXRD and XAFS investigations at high temperature, pressure, controlled gas atmosphere and ultra-fast heating

A plug-flow fixed-bed cell for synchrotron powder X-ray diffraction (PXRD) and X-ray absorption fine structure (XAFS) idoneous for the study of heterogeneous catalysts at high temperature, pressure and under gas flow is designed, constructed and demonstrated. The operating conditions up to 1000°C an...

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Bibliographic Details
Main Authors: Benjamin Bischoff, Maged F. Bekheet, Emiliano Dal Molin, Sebastian Praetz, Birgit Kanngießer, Reinhard Schomäcker, Martin Etter, Henrik S. Jeppesen, Akhil Tayal, Aleksander Gurlo, Albert Gili
Format: Article
Language:English
Published: International Union of Crystallography 2024-01-01
Series:Journal of Synchrotron Radiation
Subjects:
plug-flow fixed-bed cell
ultra-fast infra-red heating
gas–solid interactions
in situ x-ray diffraction
in situ x-ray absorption fine structure
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600577523009591

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http://scripts.iucr.org/cgi-bin/paper?S1600577523009591

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