An expeditious and consistent procedure for tetrahydrofuran (THF) drying and deoxygenation by the still apparatus

An expeditious and consistent procedure for tetrahydrofuran (THF) drying and deoxygenation by the still apparatus

Despite the availability of alternative methods for drying tetrahydrofuran (THF), the use of the still apparatus, wherein a THF solution containing Na-bezophenone ketyl is heated to reflux, remains widespread. We herein propose a set of procedures to solve the problems usually faced in applying this...

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Bibliographic Details
Main Authors: Alessandro B. C. Simas, Vera L. P. Pereira, Cleber B. Barreto Jr., Daniel L. de Sales, Leandro L. de Carvalho
Format: Article
Language:English
Published: Sociedade Brasileira de Química 2009-01-01
Series:Química Nova
Subjects:
THF
still apparatus
purification
Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422009000900042

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http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422009000900042

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