Redetermination of the crystal structure of bis(tri-2-pyridylamine)iron(II) bis(perchlorate), and a new refinement of the isotypic nickel(II) analogue: treatment of the perchlorate anion disorder

Redetermination of the crystal structure of bis(tri-2-pyridylamine)iron(II) bis(perchlorate), and a new refinement of the isotypic nickel(II) analogue: treatment of the perchlorate anion disorder

The redetermination of the structure of the title compound, [Fe(C15H12N4)2](ClO4)2, (I), confirms the structure previously reported [Kucharski et al. (1978a). Aust. J. Chem. 31, 53–56], but models the perchlorate over four sets of atomic sites, rather than using just one set of sites as in the origi...

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Bibliographic Details
Main Authors: Zouaoui Setifi, Fatima Setifi, Necmi Dege, Rafika El Ati, Christopher Glidewell
Format: Article
Language:English
Published: International Union of Crystallography 2018-05-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
polypyridyl complexes
redetermination
perchlorate anion disorder
hydrogen bonding
supramolecular assembly
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989018005601

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http://scripts.iucr.org/cgi-bin/paper?S2056989018005601

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