Preparation and X-ray structure of 2-iodoxybenzenesulfonic acid (IBS) – a powerful hypervalent iodine(V) oxidant

Preparation and X-ray structure of 2-iodoxybenzenesulfonic acid (IBS) – a powerful hypervalent iodine(V) oxidant

The selective preparation of 2-iodoxybenzenesulfonic acid (IBS, as potassium or sodium salts) by oxidation of sodium 2-iodobenzenesulfonate with Oxone or sodium periodate in water is reported. The single crystal X-ray diffraction analysis reveals a complex polymeric structure consisting of three uni...

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Bibliographic Details
Main Authors: Irina A. Mironova, Pavel S. Postnikov, Rosa Y. Yusubova, Akira Yoshimura, Thomas Wirth, Viktor V. Zhdankin, Victor N. Nemykin, Mekhman S. Yusubov
Format: Article
Language:English
Published: Beilstein-Institut 2018-07-01
Series:Beilstein Journal of Organic Chemistry
Subjects:
hypervalent iodine
iodine
2-iodoxybenzenesulfonic acid
oxidation
X-ray
Online Access:https://doi.org/10.3762/bjoc.14.159

Internet

https://doi.org/10.3762/bjoc.14.159

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