Synergy of diffraction and spectroscopic techniques to unveil the crystal structure of antimonic acid

Abstract The elusive crystal structure of the so-called ‘antimonic acid’ has been investigated by means of robust and state-of-the-art techniques. The synergic results of solid-state magic-angle spinning nuclear magnetic resonance spectroscopy and a combined Rietveld refinement from synchrotron X-ra...

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Bibliographic Details
Main Authors: S. F. Mayer, J. E. Rodrigues, I. Sobrados, J. Gainza, M. T. Fernández-Díaz, C. Marini, M. C. Asensio, J. A. Alonso
Format: Article
Language:English
Published: Nature Portfolio 2021-09-01
Series:Scientific Reports
Online Access:https://doi.org/10.1038/s41598-021-97147-0